CarbaMic acid, [2,2-diMethyl-4-oxo-1-(sulfooxy)-3-azetidinyl]-,C-(1,1-diMethylethyl) ester, ion(1-), (S)-, N,N,N-tributyl-1-butanaMiniuM

Base Information

Chemical Name:CarbaMic acid, [2,2-diMethyl-4-oxo-1-(sulfooxy)-3-azetidinyl]-,C-(1,1-diMethylethyl) ester, ion(1-), (S)-, N,N,N-tributyl-1-butanaMiniuM
CAS No.:123176-14-7
Molecular Formula:C26H53N3O7S
Molecular Weight:551.78
Hs Code.:

Synonyms:CarbaMic acid, [2,2-diMethyl-4-oxo-1-(sulfooxy)-3-azetidinyl]-,C-(1,1-diMethylethyl) ester, ion(1-), (S)-, N,N,N-tributyl-1-butanaMiniuM

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CarbaMic acid, [2,2-diMethyl-4-oxo-1-(sulfooxy)-3-azetidinyl]-,C-(1,1-diMethylethyl) ester, ion(1-), (S)-, N,N,N-tributyl-1-butanaMiniuM

Chemical Property:

PSA：133.45000
LogP:6.30550

Purity/Quality:

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Technology Process of CarbaMic acid, [2,2-diMethyl-4-oxo-1-(sulfooxy)-3-azetidinyl]-,C-(1,1-diMethylethyl) ester, ion(1-), (S)-, N,N,N-tributyl-1-butanaMiniuM

There total 9 articles about CarbaMic acid, [2,2-diMethyl-4-oxo-1-(sulfooxy)-3-azetidinyl]-,C-(1,1-diMethylethyl) ester, ion(1-), (S)-, N,N,N-tributyl-1-butanaMiniuM which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102507-38-0
C₁₀H₁₈N₂O₇S*C₅H₅N

: 2472-88-0
tetrabutylammonium sulfate

: 123176-14-7
C₁₆H₃₆N⁽¹⁺⁾*C₁₀H₁₇N₂O₇S^(1-)

Guidance literature:: With potassium dihydrogenphosphate; In dichloromethane; water; at 0 - 5 ℃; for 1h;

Reference yield:

: 32503-27-8
tetra(n-butyl)ammonium hydrogensulfate

: 102507-31-3
(3S)-3-[(t-butyloxycarbonyl)amino]-1-hydroxy-4,4-dimethyl-2-azetidinone

: 123176-14-7
C₁₆H₃₆N⁽¹⁺⁾*C₁₀H₁₇N₂O₇S^(1-)

Guidance literature:: (3S)-3-[(t-butyloxycarbonyl)amino]-1-hydroxy-4,4-dimethyl-2-azetidinone; With potassium dihydrogenphosphate; sulfur trioxide-N,N-dimethylformamide complex; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

tetra(n-butyl)ammonium hydrogensulfate; In water; ethyl acetate; at 10 ℃; for 0.333333h;

Reference yield:

: 95715-85-8
2-(tert-butoxycarbonylamino)-3-hydroxypropionic acid methyl ester

: 123176-14-7
C₁₆H₃₆N⁽¹⁺⁾*C₁₀H₁₇N₂O₇S^(1-)

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether / 1 h / -78 - 20 °C

2.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium chloride / aq. phosphate buffer; water; acetonitrile / 35 °C / pH 6 - 7

3.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 24 h / 20 °C

4.1: sulfur trioxide pyridine complex / pyridine / 2 h / 0 °C

4.2: 2 h / Reflux

5.1: 5%-palladium/activated carbon; hydrogen / methanol; water / 1 h / 2585.81 Torr

6.1: pyridine / 1.5 h / 0 - 20 °C

7.1: potassium dihydrogenphosphate / dichloromethane; water / 1 h / 0 - 5 °C

With sodium hypochlorite; potassium dihydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 5%-palladium/activated carbon; hydrogen; sulfur trioxide pyridine complex; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium chloride; In pyridine; methanol; aq. phosphate buffer; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;