2,5-Piperazinedithione,1,4-dimethyl-(9CI)

Base Information

• Chemical Name: 2,5-Piperazinedithione,1,4-dimethyl-(9CI)
• CAS No.: 86942-34-9
• Molecular Formula: C6 H10 N2 S2
• Molecular Weight: 0
• Hs Code.: 2933599090
• Mol file: 86942-34-9.mol

Synonyms:2,5-Piperazinedithione,1,4-dimethyl-(9CI);1,4-DIMETHYLPIPERAZINE-2,5-DITHIONE

Chemical Property of 2,5-Piperazinedithione,1,4-dimethyl-(9CI)

Chemical Property:

• PSA: 70.66000
• LogP: 0.39420

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-Piperazinedithione,1,4-dimethyl-(9CI)

There total 2 articles about 2,5-Piperazinedithione,1,4-dimethyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2,5-Bis(methylthio)-1,4-dimethyl-3,6-dihydropyrazindiium-bis(tetrafluoroborat) → 1,4-Dimethylpiperazin-2,5-dithion (86942-34-9)

Guidance literature:

With hydrogen sulfide; In tetrahydrofuran; pyridine; at 0 ℃;

DOI:10.1002/ardp.19933260202

Reference yield:

sarcosine anhydride (5076-82-4) → 1,4-Dimethylpiperazin-2,5-dithion (86942-34-9)

Guidance literature:

With diphosphorus pentasulfide; xylene;

Reference yield: 15.0%

4-methoxybenzenesulfonyl azide (4547-64-2) + 1,4-Dimethylpiperazin-2,5-dithion (86942-34-9) → N-(1,4-Dimethyl-5-thioxopiperazin-2-yliden)-p-methoxybenzolsulfonamid (135508-88-2) + p,p'-Dimethoxy (135508-90-6)

Guidance literature:

In xylene; for 12h; Heating;

upstream raw materials:

sarcosine anhydride

Downstream raw materials:

N-(1,4-Dimethyl-5-thioxopiperazin-2-yliden)-p-toluolsulfonamid

p,p'-Dimethyl

N-(1,4-Dimethyl-5-thioxopiperazin-2-yliden)-p-methoxybenzolsulfonamid

p,p'-Dimethoxy

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