Technology Process of 5-phenylpicolinoyl chloride
There total 7 articles about 5-phenylpicolinoyl chloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phosphorus pentachloride;
In
dichloromethane;
for 3h;
DOI:10.1007/BF00557735
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium methoxide / pyridine / 10 h / 40 °C
2: 10percent hydrochloric acid / 0.33 h
3: 58 percent / 57percent perchloric acid / acetic acid / 0.25 h
4: 51 percent / ammonium acetate, / acetic acid / 3 h / Heating
5: 76 percent / potassium permanganate, potassium hydroxide / H2O; dioxane / 3 h / 25 - 40 °C
6: phosphorus pentachloride / CH2Cl2 / 3 h
With
ammonium acetate; hydrogenchloride; potassium hydroxide; potassium permanganate; perchloric acid; phosphorus pentachloride; sodium methylate;
In
1,4-dioxane; pyridine; dichloromethane; water; acetic acid;
DOI:10.1007/BF00557735
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 76 percent / potassium permanganate, potassium hydroxide / H2O; dioxane / 3 h / 25 - 40 °C
2: phosphorus pentachloride / CH2Cl2 / 3 h
With
potassium hydroxide; potassium permanganate; phosphorus pentachloride;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1007/BF00557735
