(3R,5S)-5-(hydroxyMethyl)tetrahydrofuran-3-ol

Base Information

• Chemical Name: (3R,5S)-5-(hydroxyMethyl)tetrahydrofuran-3-ol
• CAS No.: 259539-06-5
• Molecular Formula: C₅H₁₀O₃
• Molecular Weight: 118.133
• Mol file: 259539-06-5.mol

Synonyms:(3R,5S)-5-(hydroxyMethyl)tetrahydrofuran-3-ol;(3R,5S)-5-(hydroxymethyl)tetrahydrofuran-

Chemical Property of (3R,5S)-5-(hydroxyMethyl)tetrahydrofuran-3-ol

Chemical Property:

• PSA: 49.69000
• LogP: -0.87150
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

(3R,5S)-5-(Hydroxymethyl)tetrahydrofuran-3-ol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3R,5S)-5-(hydroxyMethyl)tetrahydrofuran-3-ol

There total 20 articles about (3R,5S)-5-(hydroxyMethyl)tetrahydrofuran-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(3R,5S)-5-({[tert-butyl(diphenyl)silyl]oxy}methyl)tetrahydrofuran-3-ol (936251-85-3) → (3R,5S)-5-(hydroxymethyl)tetrahydrofuran-3-ol (164267-53-2,164267-54-3,204509-08-0,259539-06-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.tet.2007.04.047

Reference yield: 80.0%

(3S,5S)-5-({[tert-butyl(diphenyl)silyl]oxy}methyl)tetrahydrofuran-3-ol (936251-84-2) → (3S,5S)-5-(hydroxymethyl)tetrahydrofuran-3-ol (164267-53-2,164267-54-3,204509-08-0,259539-06-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.tet.2007.04.047

Reference yield: 78.0%

(2S,4S)-1,2:4,5-dianhydro-3-deoxypentitol (109905-51-3) → (3S,5R)-5-(hydroxymethyl)tetrahydrofuran-3-ol (204509-32-0,164267-53-2,164267-54-3,204509-08-0,259539-06-5)

Guidance literature:

With sodium hydroxide; at 0 - 25 ℃; for 36h;

DOI:10.1021/jo9721655

upstream raw materials:

1,4-pentadiene diepoxide

sulfuric acid

(2S,4S)-1,2:4,5-dianhydro-3-deoxypentitol

1,4-Pentadiene

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