1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

Base Information

Chemical Name:1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate
CAS No.:221141-77-1
Molecular Formula:C₁₈H₂₃NO₄
Molecular Weight:317.385
Hs Code.:
Mol file:221141-77-1.mol

Synonyms:1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

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Chemical Property of 1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

There total 3 articles about 1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161491-25-4
1-tert-butyl 3-methyl 4-(((trifluoromethyl)sulfonyl)oxy)-5,6-dihydropyridine-1,3(2H)-dicarboxylate

: 98-80-6
phenylboronic acid

: 221141-77-1
1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 3h;

Reference yield:

: 161491-25-4
1-tert-butyl 3-methyl 4-(((trifluoromethyl)sulfonyl)oxy)-5,6-dihydropyridine-1,3(2H)-dicarboxylate

: 98-80-6
phenylboronic acid

: 221141-77-1
1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

Guidance literature:: With sodium carbonate; In 1,4-dioxane; water;

Reference yield:

: 161491-24-3
methyl 1-tert-butoxycarbonyl-4-oxo-3-piperidinecarboxylate

: 221141-77-1
1-tert-butyl 3-methyl 4-phenyl-5,6-dihydropyridine-1,3(2H)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoromethylsulfonic anhydride

2: sodium carbonate / water; 1,4-dioxane

With trifluoromethylsulfonic anhydride; sodium carbonate; In 1,4-dioxane; water;