1H-Benzimidazole-1-propanamide(9CI)

Base Information

• Chemical Name: 1H-Benzimidazole-1-propanamide(9CI)
• CAS No.: 22492-17-7
• Molecular Formula: C₁₀H₁₁N₃O
• Molecular Weight: 189.217
• Hs Code.: 2933990090
• Mol file: 22492-17-7.mol

Synonyms:1H-Benzimidazole-1-propanamide(9CI);1H-benzimidazole-1-propanamide;3-(1-benzimidazolyl)propanamide;3-(benzimidazol-1-yl)propanamide;3-(benzimidazol-1-yl)propionamide;3-Benzoimidazol-1-yl-propionamide

Chemical Property of 1H-Benzimidazole-1-propanamide(9CI)

Chemical Property:

• PSA: 60.91000
• LogP: 1.61200

Purity/Quality:

99% ^*data from raw suppliers

3-(1H-1,3-benzodiazol-1-yl)propanamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1H-Benzimidazole-1-propanamide(9CI)

There total 3 articles about 1H-Benzimidazole-1-propanamide(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

benzoimidazole (51-17-2,79351-71-6) + 2-propenamide (79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5) → 3-(1H-benzo[d]imidazol-1-yl)propanamide (22492-17-7)

Guidance literature:

With triethylamine; In toluene; for 36h; Solvent; Reflux;

DOI:10.1016/j.ultsonch.2014.10.028

Reference yield:

3-(1H-benzo[d]imidazol-1-yl)propanenitrile (4414-84-0) → 3-(1H-benzo[d]imidazol-1-yl)propanamide (22492-17-7)

Guidance literature:

With sulfuric acid;

DOI:10.1021/jo01359a018

Reference yield:

→ 3-(1H-benzo[d]imidazol-1-yl)propanamide (22492-17-7)

Guidance literature:

Benzimidazol + Acrylamid in Pyridin mit Et3N(PhCH2)OH ;

upstream raw materials:

benzoimidazole

2-propenamide

3-(1H-benzo[d]imidazol-1-yl)propanenitrile

Downstream raw materials:

2-Benzimidazol-1-ylethylamine

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