5-(2-nitroethenyl)-2-Furanmethanol

Base Information

Chemical Name:5-(2-nitroethenyl)-2-Furanmethanol
CAS No.:79324-95-1
Molecular Formula:C₇H₇NO₄
Molecular Weight:169.137
Hs Code.:
DSSTox Substance ID:DTXSID901296130
Mol file:79324-95-1.mol

Synonyms:DTXSID901296130;5-(2-nitroethenyl)-2-Furanmethanol;79324-95-1

Suppliers and Price of 5-(2-nitroethenyl)-2-Furanmethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(5-[(E)-2-NITROETHENYL]FURAN-2-YL)METHANOL 95.00%
5MG
$ 495.43

AccelPharmtech
5-(2-nitroethenyl)-2-Furanmethanol 97.00%
25G
$ 4010.00

AccelPharmtech
5-(2-nitroethenyl)-2-Furanmethanol 97.00%
5G
$ 2180.00

AccelPharmtech
5-(2-nitroethenyl)-2-Furanmethanol 97.00%
1G
$ 1940.00

Total 3 raw suppliers

Chemical Property of 5-(2-nitroethenyl)-2-Furanmethanol

Chemical Property:

Vapor Pressure:0.00012mmHg at 25°C
Boiling Point:321.9°C at 760 mmHg
PKA:13.73±0.10(Predicted)
Flash Point:148.5°C
PSA：79.19000
Density:1.371g/cm³
LogP:1.54250
XLogP3:0.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:169.03750770
Heavy Atom Count:12
Complexity:186

Purity/Quality:: (5-[(E)-2-NITROETHENYL]FURAN-2-YL)METHANOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(OC(=C1)C=C[N+](=O)[O-])CO

Technology Process of 5-(2-nitroethenyl)-2-Furanmethanol

There total 2 articles about 5-(2-nitroethenyl)-2-Furanmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 67-47-0
5-hydroxymethyl-2-furfuraldehyde

: 75-52-5
nitromethane

: 79324-95-1
5-(2-nitrovinyl)furan-2-ylmethanol

Guidance literature:: With ammonium acetate; at 70 ℃; for 1h;
DOI:10.1039/c5ra19400h

Reference yield:

: 57-48-7,18875-34-8
D-Fructose

: 79324-95-1
5-(2-nitrovinyl)furan-2-ylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1: silica gel; hydrogen bromide / tetrahydrofuran / 24 h / 30 °C

2: ammonium acetate / 1 h / 70 °C

With ammonium acetate; hydrogen bromide; silica gel; In tetrahydrofuran;
DOI:10.1039/c5ra19400h