2-METHYL-1-PHENYLPROPAN-1-AMINE-HCl

Base Information

• Chemical Name: 2-METHYL-1-PHENYLPROPAN-1-AMINE-HCl
• CAS No.: 24290-47-9
• Molecular Formula: C10H16ClN
• Molecular Weight: 185.697
• Hs Code.: 2921499090
• Mol file: 24290-47-9.mol

Synonyms:2-METHYL-1-PHENYLPROPAN-1-AMINE-HCl;2-Methyl-1-phenylpropan-1-aMine hydrochloride

Chemical Property of 2-METHYL-1-PHENYLPROPAN-1-AMINE-HCl

Chemical Property:

• PSA: 26.02000
• LogP: 3.84470
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: DMSO (Slightly), Methanol (Slightly, Sonicated), Water (Slightly)

Purity/Quality:

99%, ^*data from raw suppliers

2-Methyl-1-phenylpropan-1-aminehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: α-Isopropylbenzylamine Hydrochloride is used in the synthetic preparation of arylalkylamines by addition of Grignard reagents to phosphorylaldimines.

Technology Process of 2-METHYL-1-PHENYLPROPAN-1-AMINE-HCl

There total 4 articles about 2-METHYL-1-PHENYLPROPAN-1-AMINE-HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

isopropyl phenyl ketoxime (72846-70-9,72846-71-0,6668-39-9) → 1-(phenyl)-2-(methyl)-1-propylamine hydrochloride (24290-47-9,68906-27-4)

Guidance literature:

With hydrogenchloride; copper(II) sulfate; zinc; In ethanol; water; at 20 ℃; for 3h;

DOI:10.1016/j.ejmech.2021.113190

Reference yield:

phenyl isopropyl ketone (611-70-1) → 1-(phenyl)-2-(methyl)-1-propylamine hydrochloride (24290-47-9,68906-27-4)

Guidance literature:

Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol / 6 h / 60 °C

2: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 760.05 Torr

With hydrogenchloride; hydroxylamine hydrochloride; hydrogen; sodium acetate; palladium 10% on activated carbon; In ethanol; water;

Reference yield:

N-(Diethoxyphosphoryl)benzylideneimine (180399-94-4) → 1-(phenyl)-2-(methyl)-1-propylamine hydrochloride (24290-47-9,68906-27-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / 20 °C

2: 20 percent aq. HCl / 1 h / Heating

With hydrogenchloride; In tetrahydrofuran; 1: Addition / 2: dephosphorylation;

DOI:10.1080/10426509908546190

upstream raw materials:

N-(Diethoxyphosphoryl)benzylideneimine

phenyl isopropyl ketone

isopropyl phenyl ketoxime

Downstream raw materials:

2,2-dimethyl-3-hydroxy-1-phenylpropan-1-one

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