(R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide

Base Information

Chemical Name:(R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide
CAS No.:138079-59-1
Molecular Formula:C24H28IOP
Molecular Weight:490.364
Hs Code.:
Mol file:138079-59-1.mol

Synonyms:(R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide;(3-Hydroxy-2,3-dimethylbutyl)triphenylphosphoniumiodide;[(2R)-3-Hydroxy-2,3-dimethylbutyl]triphenylphosphonium iodide

Suppliers and Price of (R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of (R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide

Chemical Property:

PSA：33.82000
LogP:1.39150

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide

There total 5 articles about (R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131249-23-5
R-4-Iodo-2,3-dimethyl-2-butanol

: 603-35-0
triphenylphosphine

: 138079-59-1
R-(+)-(2,3-Dimethyl-3-hydroxybutyl)triphenylphosphonium iodide

Guidance literature:: In acetonitrile; for 40h; Heating;
DOI:10.1016/S0040-4020(01)90124-3

Reference yield:

: 73295-12-2
(S)-2,3-dimethyl-1,3-butanediol

: 138079-59-1
R-(+)-(2,3-Dimethyl-3-hydroxybutyl)triphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / pyridine / 14 h / -4 °C

2: 85 percent / LiI / tetrahydrofuran / 0.25 h / Heating

3: 100 percent / acetonitrile / 40 h / Heating

With pyridine; lithium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4020(01)90124-3

Reference yield:

: 93748-48-2
(S)-3-hydroxy-2,3-dimethylbutyl 4-methylbenzenesulfonate

: 138079-59-1
R-(+)-(2,3-Dimethyl-3-hydroxybutyl)triphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / LiI / tetrahydrofuran / 0.25 h / Heating

2: 100 percent / acetonitrile / 40 h / Heating

With lithium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4020(01)90124-3