2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione

Base Information

Chemical Name:2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione
CAS No.:1354631-87-0
Molecular Formula:C38H56N2O2S2
Molecular Weight:636.99
Hs Code.:
Mol file:1354631-87-0.mol

Synonyms:2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione

Suppliers and Price of 2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione

Chemical Property:

PSA：100.48000
LogP:11.56320

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione

There total 4 articles about 2,5‐bis(2‐butyloctyl)‐ 3,6‐di(thiophen‐2‐ yl)pyrrolo[3,4‐ c]pyrrole‐1,4(2H,5H)‐ dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

: 85531-02-8
5-(bromomethyl)undecane

: 1354631-87-0
2,5-bis(2-butyloctyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; at 120 - 150 ℃; for 12h; Inert atmosphere;

Reference yield: 45.0%

: 3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione

: 1256345-37-5
5-(iodomethyl)undecane

: 1354631-87-0
2,5-bis(2-butyloctyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: In N,N-dimethyl-formamide; at 140 ℃; for 12h;

Reference yield:

: 1003-31-2
thiophene-2-carbonitrile

: 1354631-87-0
2,5-bis(2-butyloctyl)-3,6-di(thiophen-2-yl)pyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tert-Amyl alcohol / 4 h / 100 - 110 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 145 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; In tert-Amyl alcohol; N,N-dimethyl-formamide;
DOI:10.1021/ja301460s