5,5-Dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione

Base Information

Chemical Name:5,5-Dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione
CAS No.:21991-30-0
Molecular Formula:C20H20N2O3
Molecular Weight:336.3844
Hs Code.:
NSC Number:125823
DSSTox Substance ID:DTXSID90298752
Nikkaji Number:J1.356.465E
Wikidata:Q82040776

Synonyms:21991-30-0;5,5-dibenzyl-1,3-dimethyl-1,3-diazinane-2,4,6-trione;5,5-dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione;NSC125823;Oprea1_002329;CBDivE_010542;SCHEMBL10645739;DTXSID90298752;AKCCYMXEJXFRRN-UHFFFAOYSA-N;Cl-6155;NSC-125823;5,5-Dibenzyl-1,3-dimethyl-2,4,6(1H,3H,5H)-pyrimidinetrione

Suppliers and Price of 5,5-Dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 5,5-Dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione

Chemical Property:

Vapor Pressure:9.73E-09mmHg at 25°C
Boiling Point:462.6°Cat760mmHg
Flash Point:193.6°C
Density:1.231g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:336.14739250
Heavy Atom Count:25
Complexity:487

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=O)C(C(=O)N(C1=O)C)(CC2=CC=CC=C2)CC3=CC=CC=C3

Technology Process of 5,5-Dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione

There total 5 articles about 5,5-Dibenzyl-1,3-dimethylpyrimidine-2,4,6(1h,3h,5h)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 26371-47-1
5,5-dibenzyl-2,3,4(1H,3H,5H)pyrimidinetrione

: 77-78-1
dimethyl sulfate

: 21991-30-0
5,5-dibenzyl-1,3-dimethyl-2,3,4(1H,3H,5H)pyrimidinetrione

Guidance literature:: With sodium hydroxide; In ethanol; water; for 3h; Heating;
DOI:10.1016/S0040-4039(00)00852-2

Reference yield:

: 21544-73-0
5,5-dichloro-1,3-dimethyl-2,4,6(1H,3H,5H)-pyrimidinetrione

: 21991-30-0
5,5-dibenzyl-1,3-dimethyl-2,3,4(1H,3H,5H)pyrimidinetrione

Guidance literature:: Multi-step reaction with 2 steps

1: palladium/charcoal; acetone / Hydrogenation

2: aq.-ethanolic NaOH

With sodium hydroxide; palladium on activated charcoal; acetone;
DOI:10.1021/ja01847a008

Reference yield:

: 58378-09-9
1,3,1',3'-tetramethylhydurilic acid

: 21991-30-0
5,5-dibenzyl-1,3-dimethyl-2,3,4(1H,3H,5H)pyrimidinetrione

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅; 1,1,2,2-tetrachloro-ethane

2: palladium/charcoal; acetone / Hydrogenation

3: aq.-ethanolic NaOH

With sodium hydroxide; palladium on activated charcoal; phosphorus pentachloride; acetone; 1,1,2,2-tetrachloroethane;
DOI:10.1021/ja01847a008