7(S)-Maresin 1

Base Information

Chemical Name:7(S)-Maresin 1
CAS No.:1268720-66-6
Molecular Formula:C22H32O4
Molecular Weight:360.49
Hs Code.:
Mol file:1268720-66-6.mol

Synonyms:7(S)-Maresin 1;7-epi Maresin 1;7(S)-Maresin 1 Exclusive

Suppliers and Price of 7(S)-Maresin 1

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Cayman Chemical
7-epi Maresin 1 ≥95%
100μg
$ 496.00

Cayman Chemical
7-epi Maresin 1 ≥95%
50μg
$ 279.00

Cayman Chemical
7-epi Maresin 1 ≥95%
25μg
$ 147.00

Cayman Chemical
7-epi Maresin 1 ≥95%
10μg
$ 62.00

Total 5 raw suppliers

Chemical Property of 7(S)-Maresin 1

Chemical Property:

PSA：77.76000
LogP:4.49050

Purity/Quality:

97% ^*data from raw suppliers

7-epi Maresin 1 ≥95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 7(S)-Maresin 1

There total 17 articles about 7(S)-Maresin 1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1268720-64-4
C₃₄H₆₀O₄Si₂

: 1268720-66-6
7S-maresin 1

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/asia.201000494

Reference yield:

: 1268720-51-9
C₁₈H₂₄O₅

: 1268720-66-6
7S-maresin 1

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C

2.1: pyridine; Pd-BaSO₄; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.17 h / -78 °C

4.2: 0.67 h / -78 - 10 °C

5.1: phosphazene base-P₄-tert-butyl / hexane; acetonitrile / 2.08 h / -40 - 20 °C

6.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / -20 °C

6.2: -20 - 20 °C

7.1: sodium chlorite; sodium dihydrogenorthophosphate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; sodium chlorite; oxalyl dichloride; sodium dihydrogenorthophosphate; trimethylsilyl trifluoromethanesulfonate; Pd-BaSO₄; tetrabutyl ammonium fluoride; hydrogen; dimethyl sulfoxide; phosphazene base-P₄-tert-butyl; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 2-methyl-but-2-ene; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 4.1: Swern oxidation / 4.2: Swern oxidation / 5.1: Julia-Kocienski olefination;
DOI:10.1002/asia.201000494

Reference yield:

: 1268720-53-1
C₂₄H₃₈O₅Si

: 1268720-66-6
7S-maresin 1

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine; Pd-BaSO₄; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 0 °C / pH 7 / aq. phosphate buffer

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.17 h / -78 °C

3.2: 0.67 h / -78 - 10 °C

4.1: phosphazene base-P₄-tert-butyl / hexane; acetonitrile / 2.08 h / -40 - 20 °C

5.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / -20 °C

5.2: -20 - 20 °C

6.1: sodium chlorite; sodium dihydrogenorthophosphate / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0 - 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; sodium chlorite; oxalyl dichloride; sodium dihydrogenorthophosphate; trimethylsilyl trifluoromethanesulfonate; Pd-BaSO₄; tetrabutyl ammonium fluoride; hydrogen; dimethyl sulfoxide; phosphazene base-P₄-tert-butyl; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 2-methyl-but-2-ene; hexane; dichloromethane; water; ethyl acetate; acetonitrile; tert-butyl alcohol; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.1: Julia-Kocienski olefination;
DOI:10.1002/asia.201000494