Dehydroeburicoic acid monoacetate

Base Information

• Chemical Name: Dehydroeburicoic acid monoacetate
• CAS No.: 77035-42-8
• Molecular Formula: C₃₃H₅₀O₄
• Molecular Weight: 510.758
• Mol file: 77035-42-8.mol

Synonyms:Dehydroeburicoic acid monoacetate

Chemical Property of Dehydroeburicoic acid monoacetate

Chemical Property:

• PSA: 63.60000
• LogP: 8.13660

Purity/Quality:

≥95% ^*data from raw suppliers

Dehydroeburicoic acid monoacetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dehydroeburicoic acid monoacetate

There total 9 articles about Dehydroeburicoic acid monoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dehydroeburicoic acid (6879-05-6) + acetic anhydride (108-24-7) → dehydroeburicoic acid monoacetate (77035-42-8)

Guidance literature:

Reference yield:

3β-hydroxy-7-oxo-eburica-8,24(28)-dien-21-oic acid → 3α-acetoxy-eburica-7,9(11),24(28)-trien-21-oic acid (77035-42-8,124152-30-3)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium; pentan-1-ol

2: aluminium tert-butylate; dioxane; cyclohexanone

With 1,4-dioxane; pentan-1-ol; sodium; cyclohexanone; aluminum tri-tert-butoxide;

Reference yield:

3β-hydroxy-7-oxo-eburica-8,24(28)-dien-21-oic acid → dehydroeburicoic acid monoacetate (77035-42-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium; pentan-1-ol

With pentan-1-ol; sodium;

upstream raw materials:

3α-hydroxy-eburica-7,9(11),24(28)-trien-21-oic acid

acetic anhydride

dehydroeburiconic acid

Dehydroeburicoic acid

Refernces