1,10-PHENANTHROLINE-4,7-DICARBOXALDEHYDE

Base Information

• Chemical Name: 1,10-PHENANTHROLINE-4,7-DICARBOXALDEHYDE
• CAS No.: 130897-87-9
• Molecular Formula: C₁₄H₈N₂O₂
• Molecular Weight: 236.23
• Mol file: 130897-87-9.mol

Synonyms:1,10-PHENANTHROLINE-4,7-DICARBOXALDEHYDE;1,10-phenanthroline-4,7-dicarbaldehyde

Chemical Property of 1,10-PHENANTHROLINE-4,7-DICARBOXALDEHYDE

Chemical Property:

• Melting Point: 160 °C (decomp)(Solv: 1,4-dioxane (123-91-1); water (7732-18-5))
• Boiling Point: 503.8±45.0 °C(Predicted)
• PSA: 59.92000
• Density: 1.410±0.06 g/cm3(Predicted)
• LogP: 2.40800

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,10-PHENANTHROLINE-4,7-DICARBOXALDEHYDE

There total 2 articles about 1,10-PHENANTHROLINE-4,7-DICARBOXALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4,7-Dimethyl-1,10-phenanthroline (3248-05-3) → 4,7-dicarboxaldehyde-1,10-phenanthroline (130897-87-9)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; water; for 0.5h; Reflux;

DOI:10.1002/jhet.5570450654

Reference yield:

4,7-Dimethyl-1,10-phenanthroline (3248-05-3) → 4-formyl-7-methyl-phenanthroline + 4,7-dicarboxaldehyde-1,10-phenanthroline (130897-87-9)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; water; for 2.5h; Reflux;

DOI:10.1039/d0cc05972b

Reference yield: 68.0%

4,7-dicarboxaldehyde-1,10-phenanthroline (130897-87-9) → 1,10-phenanthroline-4,7-dicarboxylic acid (31301-31-2)

Guidance literature:

With silver nitrate; sodium hydroxide; In ethanol; water; for 16h;

DOI:10.1039/d0cc05972b

upstream raw materials:

4,7-Dimethyl-1,10-phenanthroline

Downstream raw materials:

1,10-phenanthroline-4,7-dicarboxylic acid

4,7-bis(benzoyloxymethyl)-1,10-phenanthroline