1,2-Didehydroadamantane

Base Information

Chemical Name:1,2-Didehydroadamantane
CAS No.:39257-33-5
Molecular Formula:C₁₀H₁₄
Molecular Weight:134.221
Hs Code.:
Mol file:39257-33-5.mol

Synonyms:1,2-Didehydroadamantane;Adamanta-2-ene;Adamantan-1-ene

Suppliers and Price of 1,2-Didehydroadamantane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,2-Didehydroadamantane

Chemical Property:

Melting Point:201.8 - 203.1 °C
PSA：0.00000
LogP:2.75270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-Didehydroadamantane

There total 5 articles about 1,2-Didehydroadamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2094-74-8
1-Adamantanecarbaldehyde

: 39257-33-5
Adamanten

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / 0 °C

1.2: 42 percent / hydroxylamine-o-sulfonic acid / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 0.5 h / 0 °C

2.1: -259.15 °C / Photolysis

With lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jp010907z

Reference yield:

: 39762-66-8
tricyclo<3.3.1.0^3,7>nonane-3-carbaldehyde

: 39257-33-5
Adamanten

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / cooling

1.2: hydroxylamine-O-sulfonic acid / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 1 h

1.3: 67 percent / tert-butyl hypochlorite / tetrahydrofuran; bis-(2-methoxy-ethyl) ether / 1 h

2.1: -259.15 °C / Photolysis

With lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/jp003682l