1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI)

Base Information

Chemical Name:1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI)
CAS No.:790689-62-2
Molecular Formula:C₁₁H₂₁NO₃
Molecular Weight:215.293
Hs Code.:
Mol file:790689-62-2.mol

Synonyms:1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI)

Suppliers and Price of 1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI)

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of 1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI)

There total 3 articles about 1-Pyrrolidinecarboxylicacid,2-(hydroxymethyl)-5-methyl-,1,1-dimethylethylester,(2R,5R)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74877-18-2
4-(oxiran-2-yl)butan-2-one

: 790689-62-2
(2R,5R)-2-(hydroxymethyl)-5-methylpyrrolidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / MgSO₄ / CHCl₃ / 15 h / 0 - 20 °C

2: LiAlH₄ / diethyl ether / 0 °C

3: H₂ / Pd(OH)2 / ethyl acetate

With lithium aluminium tetrahydride; hydrogen; magnesium sulfate; palladium dihydroxide; In diethyl ether; chloroform; ethyl acetate;
DOI:10.1055/s-2004-830867

Reference yield:

: 790689-59-7
((3R,5R,7aS)-7a-Methyl-3-phenyl-hexahydro-pyrrolo[2,1-b]oxazol-5-yl)-methanol

: 790689-62-2
(2R,5R)-2-(hydroxymethyl)-5-methylpyrrolidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0 °C

2: H₂ / Pd(OH)2 / ethyl acetate

With lithium aluminium tetrahydride; hydrogen; palladium dihydroxide; In diethyl ether; ethyl acetate;
DOI:10.1055/s-2004-830867