2,3,4,5-tetrafluoro-6-nitrobenzenaMine

Base Information

• Chemical Name: 2,3,4,5-tetrafluoro-6-nitrobenzenaMine
• CAS No.: 6157-98-8
• Molecular Formula: C6H2F4N2O2
• Molecular Weight: 210.088
• Hs Code.: 2921420090
• Mol file: 6157-98-8.mol

Synonyms:2,3,4,5-tetrafluoro-6-nitrobenzenaMine;2-Amino-3,4,5,6-tetrafluoronitrobenzene;2-Nitro-3,4,5,6-tetrafluoroaniline 97%;2,3,4,5-Tetrafluoro-6-nitroaniline;2-Nitro-3,4,5,6-tetrafluoroaniline97%

Chemical Property of 2,3,4,5-tetrafluoro-6-nitrobenzenaMine

Chemical Property:

• PSA: 71.84000
• LogP: 2.83780
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

2-Nitrotetrafluoroaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3,4,5-tetrafluoro-6-nitrobenzenaMine

There total 7 articles about 2,3,4,5-tetrafluoro-6-nitrobenzenaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

pentafluoronitrobenzen (880-78-4) → 4,5,6-trifluoro-2-nitro-1,3-phenylenediamine (2106-01-6) + 2,4,5-trifluoro-6-nitro-1,3-phenylenediamine (2106-00-5) + 2,3,4,5-tetrafluoro-6-nitroaniline (6157-98-8) + 2,3,5,6-tetrafluoro-4-nitroaniline (776-16-9)

Guidance literature:

With ammonia; In diethyl ether; for 18h; Ambient temperature;

DOI:10.1016/S0022-1139(96)03517-8

Reference yield: 65.0%

pentafluoronitrobenzen (880-78-4) → 2,3,4,5-tetrafluoro-6-nitroaniline (6157-98-8) + 2,3,5,6-tetrafluoro-4-nitroaniline (776-16-9)

Guidance literature:

With ammonia; In diethyl ether; for 1.5h; Ambient temperature;

DOI:10.1016/S0022-1139(96)03517-8

Reference yield: 38.0%

pentafluoronitrobenzen (880-78-4) → 2,3,4,5-tetrafluoro-6-nitroaniline (6157-98-8)

Guidance literature:

With ammonia; In diethyl ether; at 18 ℃;

DOI:10.1021/ja074211g

upstream raw materials:

2.3.4.5-Tetrafluor-6-nitro-acetanilid

pentafluoronitrobenzen

N-(2,3,4,5-tetrafluorophenyl)acetamide

Downstream raw materials:

4,5,6-trifluoro-2-nitro-1,3-phenylenediamine

2,4,5-trifluoro-6-nitro-1,3-phenylenediamine

2,3,4,5-Tetrafluoro-6-nitro-1-difluoraniline

2-NO₂-C₆F₄N(CH₃)2

Refernces

• 1、 -. "SELECTIVE POTASSIUM CHANNEL AGONISTS". Page/Page column 45. . Retrieved 2019/11/12.
• 2、 Murata, Hidenori,Miyazaki, Yuji,Inaba, Akira,Paduan-Filho, Armando,Bindilatti, Valdir,Oliveira Jr., Nei Fernandes,Delen, Zeynep,Lahti, Paul M.. "2-(4,5,6,7-Tetrafluorobenzimidazol-2-yl)-4,4,5,5-tetramethyl-4,5-dihydro-1- H-imidazole-3-oxide-1-oxyl, a hydrogen-bonded organic quasi-1D ferromagnet". . p. 186 - 194. Retrieved 2008/09/21.