1-O-Methyl-4-O,6-O-benzylidene-2,3-dideoxy-α-D-threo-2-hexenopyranose

Base Information

• Chemical Name: 1-O-Methyl-4-O,6-O-benzylidene-2,3-dideoxy-α-D-threo-2-hexenopyranose
• CAS No.: 18968-71-3
• Molecular Formula: C₁₄H₁₆O₄
• Molecular Weight: 248.279
• Mol file: 18968-71-3.mol

Synonyms:1-O-Methyl-4-O,6-O-benzylidene-2,3-dideoxy-α-D-threo-2-hexenopyranose

Chemical Property of 1-O-Methyl-4-O,6-O-benzylidene-2,3-dideoxy-α-D-threo-2-hexenopyranose

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of 1-O-Methyl-4-O,6-O-benzylidene-2,3-dideoxy-α-D-threo-2-hexenopyranose

There total 5 articles about 1-O-Methyl-4-O,6-O-benzylidene-2,3-dideoxy-α-D-threo-2-hexenopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(1aR,2S,6R,7aR,7bR)-2-Methoxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene (2880-96-8,3150-15-0,3150-16-1,3257-59-8,14187-71-4,15384-57-3,19465-13-5,32976-15-1,52885-37-7,53270-02-3,53270-03-4,65391-11-9,65391-12-0,66537-92-6,67226-04-4,71184-14-0,86420-78-2,86420-79-3,91177-51-4,91177-52-5,117708-93-7,120408-72-2) → (2R,8S,8aS)-2-Phenyl-4,4a,8,8a-tetrahydro-pyrano[3,2-d][1,3]dioxin-8-ol (5987-33-7,14125-70-3,63598-36-7,63598-38-9,84275-97-8,124579-80-2,167074-37-5) + (2R,6S,8aS)-6-Methoxy-2-phenyl-4,4a,6,8a-tetrahydro-pyrano[3,2-d][1,3]dioxine (3169-98-0,6743-71-1,18968-70-2,18968-71-3,18968-72-4,65530-27-0,65530-31-6,66512-66-1,110548-46-4,130272-53-6,132074-89-6)

Guidance literature:

With bis(cyclopentadienyl)titanium (III) chloride;

DOI:10.1021/ja00173a045

Reference yield:

→ Methyl-4,6-O-benzyliden-α-D-threo-hex-2-en-pyranosid (18968-71-3)

Guidance literature:

Erhitzen von Methyl-4,6-O-benzyliden-2-deoxy-2-iod-α-D-idopyranosid in Py.und Methansulfonylchlorid;

DOI:10.1139/v68-010

Reference yield:

→ Methyl-O-benzyliden-4,6-α-D-erythrohexan-2-pyranosid (3169-98-0,6743-71-1,18968-70-2,18968-71-3,18968-72-4,65530-27-0,65530-31-6,66512-66-1,110548-46-4,130272-53-6,132074-89-6)

Guidance literature:

Bis-p-toluolsulfonat 1, NaI, Zn;

upstream raw materials:

(1aR,2S,6R,7aR,7bR)-2-Methoxy-6-phenyl-hexahydro-1,3,5,7-tetraoxa-cyclopropa[a]naphthalene

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