2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one

Base Information

Chemical Name:2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one
CAS No.:53463-67-5
Molecular Formula:C14H8BrNO2
Molecular Weight:302.127
Hs Code.:2934999090
Mol file:53463-67-5.mol

Synonyms:2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one;2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one(SALTDATA: FREE)

Suppliers and Price of 2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(3-BROMOPHENYL)-4H-3,1-BENZOXAZIN-4-ONE 95.00%
5MG
$ 496.83

Total 6 raw suppliers

Chemical Property of 2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one

Chemical Property:

Vapor Pressure:1.37E-06mmHg at 25°C
Melting Point:118-120 °C
Boiling Point:399.4°C at 760 mmHg
PKA:1.88±0.20(Predicted)
Flash Point:195.4°C
PSA：43.10000
Density:1.56g/cm³
LogP:3.61750

Purity/Quality:

95% ^*data from raw suppliers

2-(3-BROMOPHENYL)-4H-3,1-BENZOXAZIN-4-ONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one

There total 11 articles about 2-(3-bromophenyl)-4H-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.4%

: 1711-09-7
3-bromobenzoyl chloride

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 53463-67-5
2-(3-Bromo-phenyl)-4H-3,1-benzoxazin-4-one

Guidance literature:: anthranilic acid; With pyridine; at 0 - 20 ℃; Inert atmosphere;

3-bromobenzoyl chloride; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmcl.2018.02.017

Reference yield: 68.0%

: 3-bromo-N-(2-formylphenyl)benzamide

: 53463-67-5
2-(3-Bromo-phenyl)-4H-3,1-benzoxazin-4-one

Guidance literature:: With tert.-butylhydroperoxide; cobalt(II) chloride; In acetonitrile; at 80 ℃; for 8h;
DOI:10.1002/ejoc.201501359

Reference yield: 65.0%

: 20718-17-6
2-(dimethyl(oxo)-λ⁶-sulfaneylidene)-1-phenylethan-1-one

: 3-(3-bromophenyl)-1,4,2-dioxazol-5-one

: 53463-67-5
2-(3-Bromo-phenyl)-4H-3,1-benzoxazin-4-one

Guidance literature:: With silver hexafluoroantimonate; carbonyl(η-5-cyclopentadienyl)diiodocobalt(III); In 1,2-dichloro-ethane; at 130 ℃; for 18h; Sealed tube; Schlenk technique;
DOI:10.1016/j.cclet.2020.09.020