Isoschumanniophytine

Base Information

Chemical Name:Isoschumanniophytine
CAS No.:69735-24-6
Molecular Formula:C₁₆H₉NO₅
Molecular Weight:295.251
Hs Code.:
Mol file:69735-24-6.mol

Synonyms:12-Hydroxy-9-methyl-5H,11H-pyrano[3',2':6,7][1]benzopyrano[3,4-c]pyridine-5,11-dione;Isoschumanniophytine;Schumanniophytine

Suppliers and Price of Isoschumanniophytine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
SCHUMANNIOPHYTINE 95.00%
5MG
$ 495.89

Total 0 raw suppliers

Chemical Property of Isoschumanniophytine

Chemical Property:

Melting Point:293 - 296 °C (CHCl3)
PSA：93.54000
LogP:2.46160

Purity/Quality:: SCHUMANNIOPHYTINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Isoschumanniophytine

There total 8 articles about Isoschumanniophytine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1032189-96-0
10-methoxy-schumanniophytine

: 69735-24-6
schumanniophytine

Guidance literature:: With boron trichloride; In n-heptane; dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1002/ejoc.200701116

Reference yield:

: 1013-69-0
eugenin

: 69735-24-6
schumanniophytine

Guidance literature:: Multi-step reaction with 5 steps

1: 1) K₂CO₃ / 1) acetone/DMF, 2) room temp., 16 h

2: 43 percent / Br₂ / CH₂Cl₂ / 0.33 h / Ambient temperature

3: 25 percent / (Ph₃P)2PdCl₂ / toluene / 21 h / 110 - 115 °C

4: H₂ / 10percent Pd/C / ethyl acetate / 3 h / Ambient temperature

5: CHCl₃ / 16 h / 55 °C

With hydrogen; bromine; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In dichloromethane; chloroform; ethyl acetate; toluene;
DOI:10.1021/jo00031a049

Reference yield:

: 20052-28-2
7-(Benzyloxy)-5-hydroxy-2-methyl-4H-1-benzopyran-4-one

: 69735-24-6
schumanniophytine

Guidance literature:: Multi-step reaction with 4 steps

1: 43 percent / Br₂ / CH₂Cl₂ / 0.33 h / Ambient temperature

2: 25 percent / (Ph₃P)2PdCl₂ / toluene / 21 h / 110 - 115 °C

3: H₂ / 10percent Pd/C / ethyl acetate / 3 h / Ambient temperature

4: CHCl₃ / 16 h / 55 °C

With hydrogen; bromine; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In dichloromethane; chloroform; ethyl acetate; toluene;
DOI:10.1021/jo00031a049