5-([(2-METHYL-FURAN-3-CARBONYL)-AMINO]-METHYL)-FURAN-2-CARBOXYLIC ACID

Base Information

• Chemical Name: 5-([(2-METHYL-FURAN-3-CARBONYL)-AMINO]-METHYL)-FURAN-2-CARBOXYLIC ACID
• CAS No.: 446054-20-2
• Molecular Formula: C₁₂H₁₁NO₅
• Molecular Weight: 249.223
• Hs Code.: 2932190090
• Mol file: 446054-20-2.mol

Synonyms:5-([(2-METHYL-FURAN-3-CARBONYL)-AMINO]-METHYL)-FURAN-2-CARBOXYLIC ACID;TIMTEC-BB SBB007431

Chemical Property of 5-([(2-METHYL-FURAN-3-CARBONYL)-AMINO]-METHYL)-FURAN-2-CARBOXYLIC ACID

Chemical Property:

• PSA: 92.68000
• LogP: 2.20010

Purity/Quality:

98%min ^*data from raw suppliers

5-{[(2-Methyl-furan-3-carbonyl)-amino]-methyl}-furan-2-carboxylic acid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-([(2-METHYL-FURAN-3-CARBONYL)-AMINO]-METHYL)-FURAN-2-CARBOXYLIC ACID

There total 4 articles about 5-([(2-METHYL-FURAN-3-CARBONYL)-AMINO]-METHYL)-FURAN-2-CARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H15NO5 → 5-[N-(2-methyl-3-furoyl)amino]methylfuran-2-carboxylic acid (446054-20-2)

Guidance literature:

C₁₄H₁₅NO₅; With sodium hydroxide; In ethanol; for 6h; Heating;

With hydrogenchloride; pH=2; Further stages.;

DOI:10.1134/S1070363206080251

Reference yield:

C14H21N4O3(1+)*Cl(1-) → 5-[N-(2-methyl-3-furoyl)amino]methylfuran-2-carboxylic acid (446054-20-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ethanolic HCl / Heating

2.1: Et₃N / acetonitrile / 20 °C

3.1: aq. NaOH / ethanol / 6 h / Heating

3.2: aq. HCl / pH 2

With hydrogenchloride; sodium hydroxide; triethylamine; In ethanol; acetonitrile; 1.1: Delepine reaction;

DOI:10.1134/S1070363206080251

Reference yield:

ethyl 5-(aminomethyl)furan-2-carboxylate hydrochloride → 5-[N-(2-methyl-3-furoyl)amino]methylfuran-2-carboxylic acid (446054-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Et₃N / acetonitrile / 20 °C

2.1: aq. NaOH / ethanol / 6 h / Heating

2.2: aq. HCl / pH 2

With sodium hydroxide; triethylamine; In ethanol; acetonitrile;

DOI:10.1134/S1070363206080251

upstream raw materials:

5-Chloromethyl-furan-2-carboxylic acid ethyl ester

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