Technology Process of (14β)-5α-Androstan-15-one
There total 10 articles about (14β)-5α-Androstan-15-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 4h;
DOI:10.1039/P19720002765
- Guidance literature:
-
Multi-step reaction with 7 steps
1: NaOH / tetrahydrofuran; H2O / 2 h / 20 °C
3: KOtBu / dimethylsulfoxide / 100 °C
4: Py / 0 °C
5: aq. H2CrO4 / acetone / 0 °C
6: NaHCO3 / methanol / 4 h / Heating
7: H2 / Pd-C / ethyl acetate / 4 h
With
pyridine; sodium hydroxide; potassium tert-butylate; hydrogen; chromic acid; sodium hydrogencarbonate; lithium tri-t-butoxyaluminum hydride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; water; dimethyl sulfoxide; ethyl acetate; acetone;
DOI:10.1039/P19720002765
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Py / 0 °C
2: aq. H2CrO4 / acetone / 0 °C
3: NaHCO3 / methanol / 4 h / Heating
4: H2 / Pd-C / ethyl acetate / 4 h
With
pyridine; hydrogen; chromic acid; sodium hydrogencarbonate;
palladium on activated charcoal;
In
methanol; ethyl acetate; acetone;
DOI:10.1039/P19720002765