1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol

Base Information

Chemical Name:1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol
CAS No.:170147-88-3
Molecular Formula:C₁₆H₁₇NO
Molecular Weight:239.317
Hs Code.:

Synonyms:1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol

Suppliers and Price of 1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol

There total 3 articles about 1,2,3,4-Tetrahydro-1-(phenylmethyl)-6-quinolinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.8%

: 73126-26-8
1-benzyl-6-methoxy-1,2,3,4-tetrahydroquinoline

: 170147-88-3
6-hydroxy-1-benzyl-1,2,3,4-tetrahydroquinoline

Guidance literature:: 1-benzyl-6-methoxy-1,2,3,4-tetrahydroquinoline; With water; hydrogen bromide; at 110 ℃; for 5h;

With triethylamine; In diethyl ether; at 19 ℃; for 3h;
DOI:10.1016/j.bmc.2008.11.030

Reference yield:

: 5263-87-6
6-methoxy quinoline

: 170147-88-3
6-hydroxy-1-benzyl-1,2,3,4-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; nickel-aluminum alloy / ethanol; water

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

3: boron tribromide / dichloromethane

With nickel-aluminum alloy; boron tribromide; potassium carbonate; potassium iodide; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.09.005

Reference yield:

: 120-15-0
6-methoxy-1,2,3,4-tetrahydroquinoline

: 170147-88-3
6-hydroxy-1-benzyl-1,2,3,4-tetrahydroquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 20 °C

2: boron tribromide / dichloromethane

With boron tribromide; potassium carbonate; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.09.005