2-(Benzenesulfonyl)ethyl phosphorodichloridoite

Base Information

Chemical Name:2-(Benzenesulfonyl)ethyl phosphorodichloridoite
CAS No.:98288-60-9
Molecular Formula:C₈H₉Cl₂O₃PS
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID50544025
Wikidata:Q82421000

Synonyms:2-(Benzenesulfonyl)ethyl phosphorodichloridoite;98288-60-9;DTXSID50544025

Suppliers and Price of 2-(Benzenesulfonyl)ethyl phosphorodichloridoite

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-(Benzenesulfonyl)ethyl phosphorodichloridoite

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:285.9387077
Heavy Atom Count:15
Complexity:270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)S(=O)(=O)CCOP(Cl)Cl

Technology Process of 2-(Benzenesulfonyl)ethyl phosphorodichloridoite

There total 2 articles about 2-(Benzenesulfonyl)ethyl phosphorodichloridoite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 20611-21-6
2-(phenylsulfonyl)ethanol

: 98288-60-9
2-phenylsulphonylethylphosphorodichloridite

Guidance literature:: With phosphorus trichloride; In acetonitrile; for 0.166667h; Ambient temperature;

Reference yield:

: 699-12-7
2-(phenylthio)ethanol

: 98288-60-9
2-phenylsulphonylethylphosphorodichloridite

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na₂WO₄, 2.) H₂O₂ / 1.) EtOH, H₂O, 0 deg C, 3.) EtOH, H₂O, reflux, 45 min

2: 97 percent / PCl₃ / acetonitrile / 0.17 h / Ambient temperature

With sodium tungstate; dihydrogen peroxide; phosphorus trichloride; In acetonitrile;

Reference yield:

: 98288-60-9
2-phenylsulphonylethylphosphorodichloridite

: C₄₃H₄₈N₃O₁₁PS

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.25 h / Ambient temperature

2: 90 percent / (iPr)2Et₂N / CH₂Cl₂ / 0.17 h / Ambient temperature

With (iPr)2Et₂N; In tetrahydrofuran; dichloromethane;