(3'-AMINO-BIPHENYL-3-YL)-ACETIC ACID METHYL ESTER

Base Information

• Chemical Name: (3'-AMINO-BIPHENYL-3-YL)-ACETIC ACID METHYL ESTER
• CAS No.: 1059678-65-7
• Molecular Formula: C15H15NO2
• Molecular Weight: 241.2851
• Hs Code.: 2922499990
• Mol file: 1059678-65-7.mol

Synonyms:(3'-AMINO-BIPHENYL-3-YL)-ACETIC ACID METHYL ESTER;Methyl 2-(3'-aMino-[1,1'-biphenyl]-3-yl)acetate

Chemical Property of (3'-AMINO-BIPHENYL-3-YL)-ACETIC ACID METHYL ESTER

Chemical Property:

• PSA: 52.32000
• LogP: 3.23250

Purity/Quality:

≥95% ^*data from raw suppliers

Methyl2-(3'-amino-[1,1'-biphenyl]-3-yl)acetate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3'-AMINO-BIPHENYL-3-YL)-ACETIC ACID METHYL ESTER

There total 1 articles about (3'-AMINO-BIPHENYL-3-YL)-ACETIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

3-Aminophenylboronic acid (30418-59-8,280563-63-5) + methyl 2-(3-bromophenyl)acetatee (150529-73-0) → (3'-amino-biphenyl-3-yl)-acetic acid methyl ester (1059678-65-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at 110 ℃; Inert atmosphere;

DOI:10.1021/jm800325y

Reference yield: 95.0%

benzene-1,3-disulfonyl chloride (585-47-7) + (3'-amino-biphenyl-3-yl)-acetic acid methyl ester (1059678-65-7) → C36H32N2O8S2

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/jm501449u

Reference yield: 78.0%

(3'-amino-biphenyl-3-yl)-acetic acid methyl ester (1059678-65-7) + 2-Naphthalenesulfonyl chloride (93-11-8) → C25H21NO4S (1059678-67-9)

Guidance literature:

With pyridine; In dichloromethane;

DOI:10.1021/jm800325y

upstream raw materials:

3-Aminophenylboronic acid

methyl 2-(3-bromophenyl)acetatee

Downstream raw materials:

C₂₅H₂₁NO₄S

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