(8aβ)-4aα-Phenyldecahydronaphthalene

Base Information

• Chemical Name: (8aβ)-4aα-Phenyldecahydronaphthalene
• CAS No.: 27863-63-4
• Molecular Formula: C₁₆H₂₂
• Molecular Weight: 214.351
• Mol file: 27863-63-4.mol

Synonyms:(8aβ)-4aα-Phenyldecahydronaphthalene

Chemical Property of (8aβ)-4aα-Phenyldecahydronaphthalene

Chemical Property:

• Melting Point: 49 - 50 °C
• PSA: 0.00000
• LogP: 4.68860

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (8aβ)-4aα-Phenyldecahydronaphthalene

There total 5 articles about (8aβ)-4aα-Phenyldecahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ trans-9-phenyldecalin (27863-63-4)

Guidance literature:

With ethanol; hydrazine hydrate; Erhitzen des Reaktionsprodukts mit KOH auf 130-230grad;

DOI:10.1021/ja01196a013

Reference yield:

trans-3,4,4a,5,6,8a-hexahydro-8a-phenylnaphthalene (121290-28-6) → trans-9-phenyldecalin (27863-63-4)

Guidance literature:

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jo00274a062

Reference yield:

cis-2,3,4,4a,5,6-hexahydro-2-naphthalenyl phenylcarbamate (106625-51-8,106625-53-0) → trans-9-phenyldecalin (27863-63-4)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / Pd/C

With hydrogen; palladium on activated charcoal;

DOI:10.1021/jo00274a062

upstream raw materials:

trans-3,4,4a,5,6,8a-hexahydro-8a-phenylnaphthalene

cis-2,3,4,4a,5,6-hexahydro-2-naphthalenyl phenylcarbamate

phenyllithium

Refernces