1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole
CAS No.:1130489-19-8
Molecular Formula:C18H28BN3O2Si
Molecular Weight:357.336
Hs Code.:2933998090
Mol file:1130489-19-8.mol

Synonyms:1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole

Suppliers and Price of 1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole >90%
500mg
$ 643.00

Crysdot
1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole 95+%
1g
$ 757.00

Apolloscientific
1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole
500mg
$ 486.00

AK Scientific
1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole
500mg
$ 918.00

Total 2 raw suppliers

Chemical Property of 1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole

Chemical Property:

PSA：49.17000
LogP:2.17080

Purity/Quality:

99% ^*data from raw suppliers

1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole >90% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole

There total 2 articles about 1-Benzyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 622-79-7
benzyl azide

: 159087-46-4
4,4,5,5-tetramethyl-2-trimethylsilanylethynyl-[1,3,2]dioxaborolane

: 1130489-19-8
C₆H₅CH₂C₂N₃(Si(CH₃)3)BO₂C₆H₁₂

Guidance literature:: In 1,2-dichloro-benzene; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b817052e DOI:10.1016/j.tetlet.2009.07.085

Reference yield: 84.0%

: 622-79-7
benzyl azide

: 159087-46-4
4,4,5,5-tetramethyl-2-trimethylsilanylethynyl-[1,3,2]dioxaborolane

: 1130489-19-8
C₆H₅CH₂C₂N₃(Si(CH₃)3)BO₂C₆H₁₂

: C₆H₅CH₂C₂N₃(Si(CH₃)3)BO₂C₆H₁₂

Guidance literature:: In further solvent(s); compd. reacted with BnN3 in DCB at 110°C for 24 h; regioisomer ofcycloadduct was observed by HMBC experiment; regioselectivity >98:2;
DOI:10.1039/b817052e

Reference yield: 97.0%

: 591-50-4
iodobenzene

: 1130489-19-8
C₆H₅CH₂C₂N₃(Si(CH₃)3)BO₂C₆H₁₂

: 1130489-25-6
1-benzyl-5-phenyl-4-(trimethylsilyl)-1H-1,2,3-triazole

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri tert-butylphosphoniumtetrafluoroborate; In acetonitrile; at 50 ℃; for 16h; Inert atmosphere;
DOI:10.1039/b817052e