N1,5-Dimethylbenzene-1,2-diamine

Base Information

Chemical Name:N1,5-Dimethylbenzene-1,2-diamine
CAS No.:131019-87-9
Molecular Formula:C8H12N2
Molecular Weight:136.197
Hs Code.:2921590090
DSSTox Substance ID:DTXSID60433673
Nikkaji Number:J1.802.842E
Wikidata:Q82247875
Mol file:131019-87-9.mol

Synonyms:N1,5-Dimethylbenzene-1,2-diamine;131019-87-9;2-N,4-dimethylbenzene-1,2-diamine;N'-Methyl-4-methylbenzene-1,2-diamine;MFCD19203441;N/'-Methyl-4-Methylbenzene-1,2-diaMine;N1,5-Dimethyl-1,2-benzenediamine;1,2-Benzenediamine, N2,4-dimethyl-;SCHEMBL7330774;DTXSID60433673;ICWDURLIKIKGLQ-UHFFFAOYSA-N;N,5-Dimethyl-1,2-benzenediamine;4,N2-dimethyl-benzene-1,2-diamine;AKOS006338148;DS-5491;SY114319;1-amino-4-methyl-2-(N-methylamino)benzene;CS-0018925;FT-0710704;N12938

Suppliers and Price of N1,5-Dimethylbenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N1,5-Dimethylbenzene-1,2-diamine 97%
1g
$ 260.00

Chemenu
N1,5-dimethylbenzene-1,2-diamine 95+%
1g
$ 247.00

Chemcia Scientific
4,N*2*-Dimethyl-benzene-1,2-diamine 95%
1 G
$ 350.00

BLDpharm
N1,5-Dimethylbenzene-1,2-diamine 97%
1g
$ 278.00

BLDpharm
N1,5-Dimethylbenzene-1,2-diamine 97%
100mg
$ 71.00

American Custom Chemicals Corporation
N1,5-DIMETHYLBENZENE-1,2-DIAMINE 95.00%
5MG
$ 503.15

AK Scientific
N1,5-Dimethylbenzene-1,2-diamine
250mg
$ 205.00

Total 11 raw suppliers

Chemical Property of N1,5-Dimethylbenzene-1,2-diamine

Chemical Property:

PSA：38.05000
LogP:2.27310
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
XLogP3:1.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:136.100048391
Heavy Atom Count:10
Complexity:103

Purity/Quality:

97% ^*data from raw suppliers

N1,5-Dimethylbenzene-1,2-diamine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)N)NC

Technology Process of N1,5-Dimethylbenzene-1,2-diamine

There total 12 articles about N1,5-Dimethylbenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: tetrabutylammonium p-tolylsulfamate

: O-(4-methoxybenzoyl)-N-methylhydroxylammonium trifluoromethanesulfonate

: 131019-87-9
1-amino-4-methyl-2-(N-methylamino)benzene

Guidance literature:: tetrabutylammonium p-tolylsulfamate; O-(4-methoxybenzoyl)-N-methylhydroxylammonium trifluoromethanesulfonate; With iron(II) bromide; at 30 ℃; for 4h;

With hydrogenchloride; In methanol; at 20 ℃; for 1h;
DOI:10.1021/jacs.1c05531

Reference yield:

: 446-34-4
2-fluoro-4-methyl-1-nitrobenzene

: 131019-87-9
1-amino-4-methyl-2-(N-methylamino)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: NaOAc / 80 °C

2: H₂ / Pd/C / ethanol / 2585.74 Torr

With hydrogen; sodium acetate; palladium on activated charcoal; In ethanol;
DOI:10.1016/j.bmcl.2005.07.021

Reference yield:

: 578-46-1
5-methyl-2-nitroaniline

: 131019-87-9
1-amino-4-methyl-2-(N-methylamino)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 60percent NaH in oil / dimethylformamide / 1 h / 0 °C

2: 2 g / hydrogen / 10percent Pd/C / methanol / 1520 Torr

With hydrogen; sodium hydride; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.3987/com-98-8108