3,5,7-TRICHLORO-4-FLUORO-6-IODO 1H-INDAZOLE

Base Information

• Chemical Name: 3,5,7-TRICHLORO-4-FLUORO-6-IODO 1H-INDAZOLE
• CAS No.: 100034-15-9
• Molecular Formula: C₂₅H₂₈N₄O₄S₂
• Molecular Weight: 512.654
• Mol file: 100034-15-9.mol

Synonyms:3,5,7-TRICHLORO-4-FLUORO-6-IODO 1H-INDAZOLE

Chemical Property of 3,5,7-TRICHLORO-4-FLUORO-6-IODO 1H-INDAZOLE

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5,7-TRICHLORO-4-FLUORO-6-IODO 1H-INDAZOLE

There total 3 articles about 3,5,7-TRICHLORO-4-FLUORO-6-IODO 1H-INDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C23H24N4O4S2 (100034-14-8) + dimethyl sulfate (77-78-1) → C25H28N4O4S2 (100034-15-9)

Guidance literature:

With sodium hydroxide; In water; for 1h;

Reference yield:

Toluene-2,4-bis-sulphonic acid bishydrazide (35652-57-4) → C25H28N4O4S2 (100034-15-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / ethanol / 0.33 h / Heating

2: 76 percent / NaOH / H₂O / 1 h

With sodium hydroxide; In ethanol; water;

Reference yield:

toluene-2,4-disulfonyl dichloride (2767-77-3) → C25H28N4O4S2 (100034-15-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 58 percent / hydrazine hydrate / benzene / 2 h / 0 °C

2: 78 percent / ethanol / 0.33 h / Heating

3: 76 percent / NaOH / H₂O / 1 h

With sodium hydroxide; hydrazine hydrate; In ethanol; water; benzene;

upstream raw materials:

C₂₃H₂₄N₄O₄S₂

dimethyl sulfate

toluene-2,4-disulfonyl dichloride

Toluene-2,4-bis-sulphonic acid bishydrazide

Refernces