IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo-

Base Information

Chemical Name:IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo-
CAS No.:1282516-69-1
Molecular Formula:C11H8BrIN2O
Molecular Weight:391.006
Hs Code.:2934999090
Mol file:1282516-69-1.mol

Synonyms:IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo-;9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine

Suppliers and Price of IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
9-Bromo-5,6-dihydro-2-iodoimidazo[1,2-d][1,4]benzoxazepine
1 g
$ 1127.00

Matrix Scientific
9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine 98%
500mg
$ 528.00

Matrix Scientific
9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine 98%
1g
$ 706.00

Matrix Scientific
9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine 98%
5g
$ 1652.00

Crysdot
9-Bromo-2-iodo-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine 95+%
250mg
$ 235.00

Crysdot
9-Bromo-2-iodo-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine 95+%
1g
$ 587.00

Chemenu
9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine 95+%
1g
$ 874.00

Chemenu
9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine 95+%
250mg
$ 437.00

Chemenu
9-Bromo-5,6-dihydro-2-iodo-imidazo[1,2-d][1,4]benzoxazepine 95+%
100mg
$ 284.00

Alichem
Imidazo[1,2-d][1,4]benzoxazepine,9-bromo-5,6-dihydro-2-iodo-
1g
$ 513.32

Total 12 raw suppliers

Chemical Property of IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo-

Chemical Property:

Boiling Point:491.2±55.0 °C(Predicted)
PKA:3.32±0.20(Predicted)
PSA：27.05000
Density:2.21±0.1 g/cm3(Predicted)
LogP:3.30960

Purity/Quality:

99%, ^*data from raw suppliers

9-Bromo-5,6-dihydro-2-iodoimidazo[1,2-d][1,4]benzoxazepine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo-

There total 1 articles about IMidazo[1,2-d][1,4]benzoxazepine,9-broMo-5,6-dihydro-2-iodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22532-62-3
4-bromosalicylaldehyde

: 1282516-69-1
9-bromo-2-iodo-5,6-dihydrobenzo[f ]imidazo[1,2-d][1,4]oxazepine

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / water; methanol / 2 h

2: caesium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C

3: N-iodo-succinimide / N,N-dimethyl-formamide / 48 h / 20 °C

4: ethylmagnesium bromide / diethyl ether; tetrahydrofuran / 1 h / -15 °C

With N-iodo-succinimide; ethylmagnesium bromide; ammonia; caesium carbonate; In tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide;

Reference yield: 73.0%

: 1282516-69-1
9-bromo-2-iodo-5,6-dihydrobenzo[f ]imidazo[1,2-d][1,4]oxazepine

: 17997-47-6
2-tri-n-butylstannylpyridine

: 1401303-65-8
8-bromo-2-pyridin-2-yl-4,5-dihydro-6-oxa-1,3a-diazabenzo[e]azulene

Guidance literature:: With copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 100 ℃; for 1h; Inert atmosphere; microwave irradiation;

Reference yield: 55.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1282516-69-1
9-bromo-2-iodo-5,6-dihydrobenzo[f ]imidazo[1,2-d][1,4]oxazepine

: 1282516-74-8
9-bromo-5,6-dihydrobenzo[f]imidazo[1,2-d]-[1,4]oxazepine-2-carboxylic acid

Guidance literature:: 9-bromo-2-iodo-5,6-dihydrobenzo[f ]imidazo[1,2-d][1,4]oxazepine; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 - -73 ℃; for 0.333333h;

carbon dioxide; In tetrahydrofuran; hexanes; at -78 - -55 ℃; for 1.5h;