2,6-Dibromoterephthalic acid

Base Information

Chemical Name:2,6-Dibromoterephthalic acid
CAS No.:22191-58-8
Molecular Formula:C₈H₄Br₂O₄
Molecular Weight:323.925
Hs Code.:
DSSTox Substance ID:DTXSID30596603
Nikkaji Number:J83.156E
Wikidata:Q82491904
Mol file:22191-58-8.mol

Synonyms:2,6-Dibromoterephthalic acid;22191-58-8;SCHEMBL5560892;DTXSID30596603;JQJBHBWYLZTGAL-UHFFFAOYSA-N;2,6-Dibromobenzene-1,4-dicarboxylic acid;DB-250889

Suppliers and Price of 2,6-Dibromoterephthalic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,6-Dibromoterephthalic acid

Chemical Property:

PSA：74.60000
LogP:2.60800
XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:323.84558
Heavy Atom Count:14
Complexity:244

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1Br)C(=O)O)Br)C(=O)O

Technology Process of 2,6-Dibromoterephthalic acid

There total 1 articles about 2,6-Dibromoterephthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 66788-13-4
2,6-dibromo-1,4-dimethylbenzene

: 22191-58-8
2,6-dibromoterephthalic acid

Guidance literature:: With potassium permanganate; In pyridine; water; at 110 ℃; for 12h;
DOI:10.1021/jacs.7b01650

Reference yield:

: 22191-58-8
2,6-dibromoterephthalic acid

: C₈H₂Br₂Cl₂O₂

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1021/jacs.7b01650

Reference yield:

: 22191-58-8
2,6-dibromoterephthalic acid

: 2,6-dibromoterephthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 3 h / 80 °C

2: ammonium hydroxide / 1,4-dioxane / 12 h / 20 °C

With ammonium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In 1,4-dioxane;
DOI:10.1021/jacs.7b01650