2-Methyl-5-(tributylstannyl)thiazole

Base Information

• Chemical Name: 2-Methyl-5-(tributylstannyl)thiazole
• CAS No.: 223418-75-5
• Molecular Formula: C16H31NSSn
• Molecular Weight: 388.19904
• Hs Code.: 2934100090
• Mol file: 223418-75-5.mol

Synonyms:2-Methyl-5-(tributylstannyl)thiazole

Chemical Property of 2-Methyl-5-(tributylstannyl)thiazole

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 372.293°C at 760 mmHg
• PKA: 3.44±0.10(Predicted)
• Flash Point: 178.957°C
• PSA: 41.13000
• LogP: 5.50760

Purity/Quality:

97% ^*data from raw suppliers

2-Methyl-5-(tributylstannyl)thiazole Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methyl-5-(tributylstannyl)thiazole

There total 1 articles about 2-Methyl-5-(tributylstannyl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-methylthiazole (3581-87-1,260998-77-4) + tributyltin chloride (1461-22-9) → 2-methyl-5-(tributylstannyl)thiazole (223418-75-5)

Guidance literature:

2-methylthiazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

tributyltin chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;

Reference yield:

2-methyl-5-(tributylstannyl)thiazole (223418-75-5) + C24H19ClN6O (1420620-31-0) → C28H23N7OS (1420620-37-6)

Guidance literature:

With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); In N,N-dimethyl-formamide; at 100 ℃; Inert atmosphere;

Reference yield:

2-methyl-5-(tributylstannyl)thiazole (223418-75-5) + (S)-2-amino-4-((1-(8-chloro-1-oxo-2-phenyl-1,2-dihydroisoquinolin-3-yl)ethyl)amino)pyrimidine-5-carbonitrile (1425041-70-8) → C26H21N7OS (1425042-32-5)

Guidance literature:

With palladium; In N,N-dimethyl-formamide; for 3h; Heating;

upstream raw materials:

2-methylthiazole

tributyltin chloride

Downstream raw materials:

C₂₈H₂₃N₇OS

C₂₆H₂₁N₇OS

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