3-PHENOXYPYRROLIDINE HYDROCHLORIDE

Base Information

• Chemical Name: 3-PHENOXYPYRROLIDINE HYDROCHLORIDE
• CAS No.: 21767-15-7
• Molecular Formula: C10H14ClNO
• Molecular Weight: 199.68
• Hs Code.: 2933990090
• Mol file: 21767-15-7.mol

Synonyms:3-PHENOXYPYRROLIDINE HYDROCHLORIDE;3-Phenoxypyrrolidine HCl

Chemical Property of 3-PHENOXYPYRROLIDINE HYDROCHLORIDE

Chemical Property:

• PSA: 21.26000
• LogP: 2.55810
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Phenoxypyrrolidine hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-PHENOXYPYRROLIDINE HYDROCHLORIDE

There total 1 articles about 3-PHENOXYPYRROLIDINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl 3-phenoxypyrrolidine-1-carboxylate (83220-74-0) → 3-phenoxypyrrolidine hydrochloride (21767-15-7,1366664-52-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; Cooling;

Reference yield: 68.0%

3-phenoxypyrrolidine hydrochloride (21767-15-7,1366664-52-9) + (E)-3-(7-oxo-5,6,7,8-tetrahydro-1,8-naphthyridin-3-yl)acrylic acid hydrochloride → 6-[(1E)-3-oxo-3-(3-phenoxypyrrolidin-1-yl)prop-1-en-1-yl]-3,4-dihydro-1,8-naphthyridin-2(1H)-one (1309205-48-8)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

3-phenoxypyrrolidine hydrochloride (21767-15-7,1366664-52-9) + 5-(8-bromoimidazo[1,2-b]pyridazin-6-yl)pyrimidine-2,4(1H,3H)-dione + trifluoroacetic acid (76-05-1) → 5-(8-(3-phenoxypyrrolidin-1-yl)imidazo[1,2-b]pyridazin-6-yl)pyrimidine-2,4(1H,3H)-dione trifluoroacetate

Guidance literature:

3-phenoxypyrrolidine hydrochloride; 5-(8-bromoimidazo[1,2-b]pyridazin-6-yl)pyrimidine-2,4(1H,3H)-dione; With N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 65 ℃; for 1h;

trifluoroacetic acid; In water; acetonitrile;

upstream raw materials:

tert-butyl 3-phenoxypyrrolidine-1-carboxylate

Downstream raw materials:

6-[(1E)-3-oxo-3-(3-phenoxypyrrolidin-1-yl)prop-1-en-1-yl]-3,4-dihydro-1,8-naphthyridin-2(1H)-one

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