N-[3',6'-Bis(ethylaMino)-2',7'-diMethyl-3-oxospiro[1H-isoindole-1,9'-[9H]xanthen]-2(3H)-yl]-N'-phenylthiourea

Base Information

• Chemical Name: N-[3',6'-Bis(ethylaMino)-2',7'-diMethyl-3-oxospiro[1H-isoindole-1,9'-[9H]xanthen]-2(3H)-yl]-N'-phenylthiourea
• CAS No.: 885481-03-8
• Molecular Formula: C33H33N5O2S
• Molecular Weight: 563.723
• Mol file: 885481-03-8.mol

Synonyms:N-[3',6'-Bis(ethylaMino)-2',7'-diMethyl-3-oxospiro[1H-isoindole-1,9'-[9H]xanthen]-2(3H)-yl]-N'-phenylthiourea;RhodaMine-6G N-Phenyl-thioseMicarbazide

Chemical Property of N-[3',6'-Bis(ethylaMino)-2',7'-diMethyl-3-oxospiro[1H-isoindole-1,9'-[9H]xanthen]-2(3H)-yl]-N'-phenylthiourea

Chemical Property:

• PSA: 116.79000
• LogP: 7.61730

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Rhodamine-6GN-Phenyl-thiosemicarbazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Rhodamine-6G N-Phenyl-thiosemicarbazide is a selective fluorescent sensor based on Rhodamine for imaging mercury in living cells.

Technology Process of N-[3',6'-Bis(ethylaMino)-2',7'-diMethyl-3-oxospiro[1H-isoindole-1,9'-[9H]xanthen]-2(3H)-yl]-N'-phenylthiourea

There total 2 articles about N-[3',6'-Bis(ethylaMino)-2',7'-diMethyl-3-oxospiro[1H-isoindole-1,9'-[9H]xanthen]-2(3H)-yl]-N'-phenylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

rhodamine hydrazide (932013-08-6) + phenyl isothiocyanate (103-72-0) → C33H33N5O2S (885481-03-8)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 6h;

DOI:10.1021/ja054855t

Reference yield:

rhodamine 6G (106627-60-5) → C33H33N5O2S (885481-03-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / hydrazine monohydrate / methanol / 6 h / Heating

2: 90 percent / dimethylformamide / 6 h / 20 °C

With hydrazine hydrate; In methanol; N,N-dimethyl-formamide;

DOI:10.1021/ja054855t

Reference yield: 98.0%

C33H33N5O2S (885481-03-8) → {5-[2-(6-ethylamino-3-ethylimino-2,7-dimethyl-3H-xanthen-9-yl)-phenyl]-[1,3,4]oxadiazol-2-yl}-phenyl-amine

Guidance literature:

With mercury(II) perchlorate; In acetonitrile; at 20 ℃; for 0.0833333h;

DOI:10.1021/ja054855t

upstream raw materials:

rhodamine hydrazide

phenyl isothiocyanate

rhodamine 6G

Downstream raw materials:

C₃₃H₃₁N₅O₂

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