2-(Benzyloxycarbonylamino)ethylboronic acid

Base Information

• Chemical Name: 2-(Benzyloxycarbonylamino)ethylboronic acid
• CAS No.: 4540-87-8
• Molecular Formula: C10H14BNO4
• Molecular Weight: 223.036
• Hs Code.: 2931900090
• Mol file: 4540-87-8.mol

Synonyms:2-(Benzyloxycarbonylaminol)ethylboronic acid;2-(Benzyloxycarbonylamino)ethylboronic acid;Benzyl N-[2-(dihydroxyboranyl)ethyl]carbamate;2-benzyl carbaMate ethyl boronic acid

Chemical Property of 2-(Benzyloxycarbonylamino)ethylboronic acid

Chemical Property:

• PKA: 10.02±0.43(Predicted)
• PSA: 78.79000
• Density: 1.208±0.06 g/cm3(Predicted)
• LogP: 0.77650
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

2-(Benzyloxycarbonylamino)ethylboronicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(Benzyloxycarbonylamino)ethylboronic acid

There total 1 articles about 2-(Benzyloxycarbonylamino)ethylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl N-vinylcarbamate (84713-20-2) → (2-[[(benzyloxy)carbonyl]amino]ethyl)boronic acid (4540-87-8)

Guidance literature:

Multistep reaction; (i) B₂H₆, THF (ii) MeOH, (iii) H₂O;

DOI:10.1021/ja00955a019

Reference yield: 72.0%

1,1-Diphenylethylene (530-48-3) + (2-[[(benzyloxy)carbonyl]amino]ethyl)boronic acid (4540-87-8) → C24H25NO2

Guidance literature:

With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; In N,N-dimethyl acetamide; at 20 ℃; for 20h; Irradiation;

DOI:10.1021/acscatal.1c02823

Reference yield: 52.0%

4-Methoxystyrene (637-69-4,24936-44-5) + (2-[[(benzyloxy)carbonyl]amino]ethyl)boronic acid (4540-87-8) → (±)-benzyl 2-(4-methoxyphenyl)pyrrolidine-1-carboxylate

Guidance literature:

With manganese(IV) oxide; C₁₂H₈N₂*2CF₃O₃S^(1-)*Cu⁽²⁺⁾; In 1,2-dichloro-ethane; at 105 ℃; for 24h; Inert atmosphere; Sealed tube; Sonication; Molecular sieve;

DOI:10.1021/acs.orglett.6b01259

upstream raw materials:

benzyl N-vinylcarbamate

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