N-[(1S,2S)-2-aMino-1,2-diphenylethyl]-4-(trifluoroMethyl)-BenzenesulfonaMide

Base Information

• Chemical Name: N-[(1S,2S)-2-aMino-1,2-diphenylethyl]-4-(trifluoroMethyl)-BenzenesulfonaMide
• CAS No.: 410096-73-0
• Molecular Formula: C21H19F3N2O2S
• Molecular Weight: 420.4479696
• Mol file: 410096-73-0.mol

Synonyms:N-[(1S,2S)-2-aMino-1,2-diphenylethyl]-4-(trifluoroMethyl)-BenzenesulfonaMide

Chemical Property of N-[(1S,2S)-2-aMino-1,2-diphenylethyl]-4-(trifluoroMethyl)-BenzenesulfonaMide

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

97% ^*data from raw suppliers

N-[(1S,2S)-2-Amino-1,2-diphenylethyl]-4-(trifluoromethyl)benzenesulfonamide 95%+ ^*data from reagent suppliers

Safty Information:

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Technology Process of N-[(1S,2S)-2-aMino-1,2-diphenylethyl]-4-(trifluoroMethyl)-BenzenesulfonaMide

There total 2 articles about N-[(1S,2S)-2-aMino-1,2-diphenylethyl]-4-(trifluoroMethyl)-BenzenesulfonaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

4-trifluorophenylsulfonyl chloride (2991-42-6) + (S,S)-1,2-diphenyl-1,2-diaminoethane (29841-69-8) → (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-4-trifluoromethyl-benzenesulfonamide (410096-73-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h; Cooling with ice;

DOI:10.1039/c0ob00757a

Reference yield: 82.0%

4-trifluorophenylsulfonyl chloride (2991-42-6) + (R,R)-1,2-diphenylethylenediamine (35132-20-8) → N-((1R,2R)-2-amino-1,2-diphenylethyl)-4-(trifluoromethyl)benzenesulfonamide (1105576-13-3,410096-73-0)

Guidance literature:

In dichloromethane; 1,2-dichloro-ethane; at 0 ℃; for 4h;

Reference yield: 93.7%

[osmium(II)dichloride(η6-p-cymene)]2 + N-((1R,2R)-2-amino-1,2-diphenylethyl)-4-(trifluoromethyl)benzenesulfonamide (1105576-13-3,410096-73-0) → C31H31F3N2O2OsS

Guidance literature:

With potassium hydroxide; In dichloromethane; water;

DOI:10.1021/acs.organomet.1c00358

upstream raw materials:

4-trifluorophenylsulfonyl chloride

(S,S)-1,2-diphenyl-1,2-diaminoethane

(R,R)-1,2-diphenylethylenediamine

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