as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-

Base Information

Chemical Name:as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-
CAS No.:69466-72-4
Molecular Formula:C12H13N3O2S
Molecular Weight:263.32
Hs Code.:
DSSTox Substance ID:DTXSID40219654
Wikidata:Q83096623

Synonyms:BRN 0658102;as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-;69466-72-4;5-(3,4-Dimethoxyphenyl)-3-(methylthio)-as-triazine;1,2,4-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-;SCHEMBL11337048;DTXSID40219654;LS-155358

Suppliers and Price of as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-

Chemical Property:

Vapor Pressure:8.92E-08mmHg at 25°C
Boiling Point:447.4°Cat760mmHg
Flash Point:224.4°C
Density:1.29g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:263.07284784
Heavy Atom Count:18
Complexity:258

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2=CN=NC(=N2)SC)OC

Technology Process of as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)-

There total 3 articles about as-Triazine, 5-(3,4-dimethoxyphenyl)-3-(methylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.7%

: 15462-03-0
3',4'-dimethoxyphenylglyoxal

: 35600-34-1
S-methyl isothiosemicarbazide hydroiodide

: 69466-72-4
5-(3,4-dimethoxyphenyl)-3-(methylthio)-1,2,4-triazine

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; for 2h; regioselective reaction; Reflux;
DOI:10.1016/j.bmc.2013.11.011

Reference yield:

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 69466-72-4
5-(3,4-dimethoxyphenyl)-3-(methylthio)-1,2,4-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide / 1,4-dioxane; water / 5 h / Reflux

2: sodium hydrogencarbonate / water; ethanol / 2 h / Reflux

With selenium(IV) oxide; sodium hydrogencarbonate; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.bmc.2013.11.011