2-(Di-1-adamantylphosphino)phenylpiperidine

Base Information

• Chemical Name: 2-(Di-1-adamantylphosphino)phenylpiperidine
• CAS No.: 1237588-13-4
• Molecular Formula: C31H44NP
• Molecular Weight: 461.671
• Mol file: 1237588-13-4.mol

Synonyms:2-(Di-1-adamantylphosphino)phenylpiperidine;Di(1-adamantyl)-1-piperidinylphenylphosphine;Bis(adamant-1-yl)(2-piperidinophenyl)phosphine

Chemical Property of 2-(Di-1-adamantylphosphino)phenylpiperidine

Chemical Property:

• Melting Point: 225-230℃
• PSA: 16.83000
• LogP: 7.78670

Purity/Quality:

95% ^*data from raw suppliers

Di(1-adamantyl)-1-piperidinylphenylphosphine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(Di-1-adamantylphosphino)phenylpiperidine

There total 1 articles about 2-(Di-1-adamantylphosphino)phenylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

1-(2-bromophenyl)piperidine (82212-00-8,156808-79-6) + di-1-adamantylphosphine (131211-27-3) → N-[2-(di(1-adamantyl)phosphino)phenyl]piperidine (1237588-13-4)

Guidance literature:

With 1,1'-bis(diisopropylphosphino)ferrocene; palladium diacetate; sodium t-butanolate; In toluene; at 110 ℃;

DOI:10.1002/anie.201000526

Reference yield: 95.0%

N-[2-(di(1-adamantyl)phosphino)phenyl]piperidine (1237588-13-4) + (η3-indenyl)2(μ-OTf)2Pd2 → (η3-indenyl)Pd(PipDalPhos)(OTf)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield: 87.0%

chloro(dimethylsulfide) gold(I) (29892-37-3) + N-[2-(di(1-adamantyl)phosphino)phenyl]piperidine (1237588-13-4) → chloro[2-(di-1-adamantylphosphino)phenyl-piperidine]gold(I)

Guidance literature:

In dichloromethane; at -20 - 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/acs.orglett.9b03082

upstream raw materials:

1-(2-bromophenyl)piperidine

di-1-adamantylphosphine

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