4-(1,3-Dimethyl-2,4,6-trioxohexahydropyrimidin-5-ylidenemethyl)benzeneboronic acid pinacol ester

Base Information

• Chemical Name: 4-(1,3-Dimethyl-2,4,6-trioxohexahydropyrimidin-5-ylidenemethyl)benzeneboronic acid pinacol ester
• CAS No.: 1218790-48-7
• Molecular Formula: C₁₉H₂₃BN₂O₅
• Molecular Weight: 370.213
• Hs Code.: 2934999090
• Mol file: 1218790-48-7.mol

Synonyms:4-(1,3-Dimethyl-2,4,6-trioxohexahydropyrimidin-5-ylidenemethyl)benzeneboronic acid pinacol ester;1,3-Dimethyl-5-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzylidene]-pyrimidine-2,4,6-tr;1,3-Dimethyl-5-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzylidene]-pyrimidine-2,4,6-trione;1-(5-Benzylidene-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione)-4-boronic acid pinacol ester 97%

Chemical Property of 4-(1,3-Dimethyl-2,4,6-trioxohexahydropyrimidin-5-ylidenemethyl)benzeneboronic acid pinacol ester

Chemical Property:

• Melting Point: 196-200 °C
• PSA: 76.15000
• LogP: 1.29540

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,3-Dimethyl-5-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzylidene]pyrimidine-2,4,6-trione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(1,3-Dimethyl-2,4,6-trioxohexahydropyrimidin-5-ylidenemethyl)benzeneboronic acid pinacol ester

There total 1 articles about 4-(1,3-Dimethyl-2,4,6-trioxohexahydropyrimidin-5-ylidenemethyl)benzeneboronic acid pinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-dimethylbarbituric acid (769-42-6) + 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde (128376-64-7) → 1,3-dimethyl-5-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzylidene)pyrimidine-2,4,6(1H,3H,5H)-trione (1218790-48-7)

Guidance literature:

In water; at 100 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c6cc07819b

upstream raw materials:

1,3-dimethylbarbituric acid

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

Refernces