4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro-

Base Information

Chemical Name:4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro-
CAS No.:128099-82-1
Molecular Formula:C₁₁H₇ClN₂O₄
Molecular Weight:266.641
Hs Code.:
Mol file:128099-82-1.mol

Synonyms:4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro-

Suppliers and Price of 4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro-

Chemical Property:

PSA：83.20000
LogP:1.57200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro-

There total 7 articles about 4H-Pyrrolo[3,2,1-ij]quinoline-4,6(5H)-dione, 5-chloro-1,2-dihydro-5-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 128099-81-0
6-hydroxy-5-nitro-1,2-dihydro-4H-pyrrolo<3,2,1-ij>quinolin-4-one

: 128099-82-1
5-chloro-5-nitro-1,2,5,6-tetrahydro-4H-pyrrolo<3,2,1-ij>quinoline-4,6-dione

Guidance literature:: With sulfuryl dichloride; In 1,4-dioxane; Heating;
DOI:10.1002/jhet.5570260609

Reference yield:

: 496-15-1
1-indoline

: 128099-82-1
5-chloro-5-nitro-1,2,5,6-tetrahydro-4H-pyrrolo<3,2,1-ij>quinoline-4,6-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / 240 °C

2: 74 percent / AlCl₃, NaCl / 0.17 h / 205 °C

3: 82 percent / nitric acid / acetic acid / 1.) 50 - 60 deg C, 2.) 95 deg C, 3 min

4: 63 percent / sulfuryl chloride / dioxane / Heating

With aluminium trichloride; sulfuryl dichloride; nitric acid; sodium chloride; In 1,4-dioxane; acetic acid;
DOI:10.1002/jhet.5570260609

Reference yield:

: 53147-85-6
6-hydroxy-1,2-dihydro-4H-pyrrolo<3,2,1-ij>quinolin-4-one

: 128099-82-1
5-chloro-5-nitro-1,2,5,6-tetrahydro-4H-pyrrolo<3,2,1-ij>quinoline-4,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / nitric acid / acetic acid / 1.) 50 - 60 deg C, 2.) 95 deg C, 3 min

2: 63 percent / sulfuryl chloride / dioxane / Heating

With sulfuryl dichloride; nitric acid; In 1,4-dioxane; acetic acid;
DOI:10.1002/jhet.5570260609