3-aMino-2-oxo-1-Pyrrolidineacetic acid

Base Information

• Chemical Name: 3-aMino-2-oxo-1-Pyrrolidineacetic acid
• CAS No.: 77591-07-2
• Molecular Formula: C6H10N2O3
• Molecular Weight: 158.1552
• Mol file: 77591-07-2.mol

Synonyms:3-aMino-2-oxo-1-Pyrrolidineacetic acid

Chemical Property of 3-aMino-2-oxo-1-Pyrrolidineacetic acid

Chemical Property:

• PSA: 83.63000
• LogP: -0.73120

Purity/Quality:

3-amino-2-oxo-1-Pyrrolidineaceticacid 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-aMino-2-oxo-1-Pyrrolidineacetic acid

There total 2 articles about 3-aMino-2-oxo-1-Pyrrolidineacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-<(benzyloxycarbonyl)methyl>-3-amino-2-pyrrolidone trifluoroacetate (99707-67-2) → (+/-)-1-(carboxymethyl)-3-amino-2-pyrrolidone (77591-07-2,179605-47-1,179605-48-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; water; under 2068.6 Torr; Yield given;

DOI:10.1021/jm00152a014

Reference yield:

1-<(benzyloxycarbonyl)methyl>-3-<(tert-butoxycarbonyl)amino>-2-pyrrolidone (99707-37-6) → (+/-)-1-(carboxymethyl)-3-amino-2-pyrrolidone (77591-07-2,179605-47-1,179605-48-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol; H₂O / 2068.6 Torr

With hydrogen; palladium on activated charcoal; In methanol; water;

DOI:10.1021/jm00152a014

Reference yield:

C21H14F2N6 + (+/-)-1-(carboxymethyl)-3-amino-2-pyrrolidone (77591-07-2,179605-47-1,179605-48-2) → C26H20F2N8O3

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In methanol; 1,2-dichloro-ethane; at 40 ℃; for 2h;

upstream raw materials:

1-<(benzyloxycarbonyl)methyl>-3-amino-2-pyrrolidone trifluoroacetate

1-<(benzyloxycarbonyl)methyl>-3-<(tert-butoxycarbonyl)amino>-2-pyrrolidone

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