2-{[5-(anilinomethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}acetohydrazide

Base Information

• Chemical Name: 2-{[5-(anilinomethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}acetohydrazide
• CAS No.: 680594-25-6
• Molecular Formula: C17H18N6OS
• Molecular Weight: 354.42942
• Hs Code.: 2933990090
• Mol file: 680594-25-6.mol

Synonyms:2-{[5-(anilinomethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}acetohydrazide

Chemical Property of 2-{[5-(anilinomethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}acetohydrazide

Chemical Property:

• PSA: 123.16000
• LogP: 3.12560

Purity/Quality:

98%min ^*data from raw suppliers

2-((4-Phenyl-5-((phenylamino)methyl)-4H-1,2,4-triazol-3-yl)thio)acetohydrazide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-{[5-(anilinomethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}acetohydrazide

There total 5 articles about 2-{[5-(anilinomethyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

ethyl [4-phenyl-5-(N-phenylamino)methyl-1,2,4-triazol-3-yl]thioglycolate (680594-23-4) → [4-phenyl-5-(N-phenylamino)methyl-1,2,4-triazol-3-yl]thioglycolylhydrazide (680594-25-6)

Guidance literature:

With hydrazine hydrate; In ethanol; for 3h; Heating;

Reference yield:

N-phenylaminoacetyl hydrazide (29111-46-4) → [4-phenyl-5-(N-phenylamino)methyl-1,2,4-triazol-3-yl]thioglycolylhydrazide (680594-25-6)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 85 percent / ethanol / 1 h / Heating

2.1: 78 percent / aq. NaOH / 3 h / Heating

3.1: NaOH / ethanol / 0.75 h / Heating

3.2: 68 percent / ethanol / 4 h / Heating

4.1: 79 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;

Reference yield:

phenyl isothiocyanate (103-72-0) → [4-phenyl-5-(N-phenylamino)methyl-1,2,4-triazol-3-yl]thioglycolylhydrazide (680594-25-6)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 85 percent / ethanol / 1 h / Heating

2.1: 78 percent / aq. NaOH / 3 h / Heating

3.1: NaOH / ethanol / 0.75 h / Heating

3.2: 68 percent / ethanol / 4 h / Heating

4.1: 79 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;

upstream raw materials:

ethyl [4-phenyl-5-(N-phenylamino)methyl-1,2,4-triazol-3-yl]thioglycolate

N-phenylaminoacetyl hydrazide

phenyl isothiocyanate

5-mercapto-4-phenyl-3-(N-phenylamino)methyl-1,2,4-triazole

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