2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamine hydrochloride

Base Information

• Chemical Name: 2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamine hydrochloride
• CAS No.: 1190044-24-6
• Molecular Formula: C5H13ClN2O2S
• Molecular Weight: 200.689
• Hs Code.: 2934100090
• Mol file: 1190044-24-6.mol

Synonyms:2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamine hydrochloride;2-(2-Aminoethyl)isothiazolidine 1,1-dioxide hydrochloride

Chemical Property of 2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamine hydrochloride

Chemical Property:

• PSA: 71.78000
• LogP: 1.50160

Purity/Quality:

97% ^*data from raw suppliers

2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamine hydrochloride

There total 2 articles about 2-(1,1-Dioxo-isothiazolidin-2-yl)-ethylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl (2-(1,1-dioxidoisothiazolidin-2-yl)ethyl)carbamate → 2-(2-aminoethyl)isothiazolidine-1,1-dioxide hydrochloride (1190044-24-6)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 15 - 30 ℃;

Reference yield:

tert‐butyl N‐[2‐(3‐chloropropanesulfonamido)ethyl]carbamate → 2-(2-aminoethyl)isothiazolidine-1,1-dioxide hydrochloride (1190044-24-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Cooling with ice

2: hydrogenchloride / ethyl acetate / 4 h / 20 °C

With hydrogenchloride; sodium hydride; In ethyl acetate; N,N-dimethyl-formamide;

Reference yield: 29.0%

2-(2-aminoethyl)isothiazolidine-1,1-dioxide hydrochloride (1190044-24-6) + N-[3-(chloromethyl)-8-methylquinolin-7-yl]-4-(cyclopropylmethoxy)benzamide hydrochloride (1018856-64-8) → 4-(cyclopropylmethoxy)-N-[3-({[2-(1,1-dioxidoisothiazolidin-2-yl)ethyl]amino}methyl)-8-methylquinolin-7-yl]benzamide (1190043-79-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 4h;

Downstream raw materials:

4-(cyclopropylmethoxy)-N-[3-({[2-(1,1-dioxidoisothiazolidin-2-yl)ethyl]amino}methyl)-8-methylquinolin-7-yl]benzamide

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