tributylstannyl p-hydroxybenzoate

Base Information

• Chemical Name: tributylstannyl p-hydroxybenzoate
• CAS No.: 7414-81-5
• Molecular Formula: C19H32 O3 Sn
• Molecular Weight: 427.171
• Mol file: 7414-81-5.mol

Synonyms:Phenol,4-[[(tributylstannyl)oxy]carbonyl]- (9CI); Tin,tributyl[(p-hydroxybenzoyl)oxy]- (7CI,8CI); Benzoic acid, p-hydroxy-,tributyltin deriv. (8CI); Tributylstannyl 4-hydroxybenzoate; Tributyltinp-hydroxybenzoate

Chemical Property of tributylstannyl p-hydroxybenzoate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tributylstannyl p-hydroxybenzoate

There total 2 articles about tributylstannyl p-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(tri-n-butyltin)oxide (56-35-9) + 4-hydroxy-benzoic acid (99-96-7) → (C4H9)3SnOOCC6H4OH-4 (7414-81-5)

Guidance literature:

In toluene; byproducts: H2O; 1:2 mole ratio; azeotropic removal of water;

Reference yield:

→ (C4H9)3SnOOCC6H4OH-4 (7414-81-5)

Guidance literature:

2O, p-Hydroxybenzoesaeure;

DOI:10.1016/S0022-328X(00)93542-3

Reference yield: 74.6%

2-(acetoxymethyl)-6-bromotetrahydro-2H-pyran-3,4,5-triyl triacetate (529493-92-3) + (C4H9)3SnOOCC6H4OH-4 (7414-81-5) → C5OH5CH2(OOCCH3)4OOCC6H4OH-4 + tributyltin bromide (1461-23-0)

Guidance literature:

With (N(C₄H₉)4)Br; In 1,2-dichloro-ethane; 1:1:1 mole ratio;

upstream raw materials:

bis(tri-n-butyltin)oxide

4-hydroxy-benzoic acid

Downstream raw materials:

tributyltin bromide