3-Hydroxxy-α-calacorene

Base Information

Chemical Name:3-Hydroxxy-α-calacorene
CAS No.:60263-12-9
Molecular Formula:C₁₅H₂₀O
Molecular Weight:216.323
Hs Code.:
Mol file:60263-12-9.mol

Synonyms:1,2-Dihydro-1-isopropyl-4,7-dimethyl-6-naphthol;3-Hydroxxy-α-calacorene;5,6-Dihydro-5-isopropyl-3,8-dimethyl-2-naphthol

Suppliers and Price of 3-Hydroxxy-α-calacorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(±)-7-Hydroxy-3,4-dihydrocadalin
10mg
$ 495.00

Total 2 raw suppliers

Chemical Property of 3-Hydroxxy-α-calacorene

Chemical Property:

Melting Point:108 °C (pentane)
Boiling Point:342.0±31.0 °C(Predicted)
PKA:10.53±0.40(Predicted)
PSA：20.23000
Density:1.009±0.06 g/cm3(Predicted)
LogP:4.24720

Purity/Quality:

95%+ or 98%+ ^*data from raw suppliers

(±)-7-Hydroxy-3,4-dihydrocadalin ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses (±)-7-Hydroxy-3,4-dihydrocadalin is one of the main components of essential oil of flowers of H. inuloides (Asteraceae).

Technology Process of 3-Hydroxxy-α-calacorene

There total 5 articles about 3-Hydroxxy-α-calacorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78310-06-2
1,2-Dihydro-7-hydroxy-4-isopropyl-6-methyl-1-naphthalincarbonsaeure-ethylester

: 60263-12-9
7-hydroxy-3,4-dihydrocadalin

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / H₂ / 10percent Pd/BaSO₄ / ethanol

2: 93.3 percent / NaH / toluene / 16 h / Ambient temperature

3: LiAlH₄ / diethyl ether

4: 1) NaH / 1) ether, r.t., 30 min, 2) ether, 45 min

5: 2) conc. HCl / 1) 220 deg C, 80 Torr, 1 h, 2) MeOH, reflux, 1 h

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium hydride; Pd-BaSO₄; In diethyl ether; ethanol; toluene;

Reference yield:

: 78310-10-8
(1S,4S)-4-Isopropyl-7-methoxymethoxy-6-methyl-1,2,3,4-tetrahydro-naphthalene-1-carboxylic acid ethyl ester

: 60263-12-9
7-hydroxy-3,4-dihydrocadalin

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether

2: 1) NaH / 1) ether, r.t., 30 min, 2) ether, 45 min

3: 2) conc. HCl / 1) 220 deg C, 80 Torr, 1 h, 2) MeOH, reflux, 1 h

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; In diethyl ether;

Reference yield:

: 78310-07-3,78310-08-4
1,2,3,4-Tetrahydro-7-hydroxy-4β-isopropyl-6-methyl-1β-naphthalincarbonsaeure-ethylester

: 60263-12-9
7-hydroxy-3,4-dihydrocadalin

Guidance literature:: Multi-step reaction with 4 steps

1: 93.3 percent / NaH / toluene / 16 h / Ambient temperature

2: LiAlH₄ / diethyl ether

3: 1) NaH / 1) ether, r.t., 30 min, 2) ether, 45 min

4: 2) conc. HCl / 1) 220 deg C, 80 Torr, 1 h, 2) MeOH, reflux, 1 h

With hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; In diethyl ether; toluene;