5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose

Base Information

Chemical Name:5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose
CAS No.:871347-98-7
Molecular Formula:C17H24O6
Molecular Weight:324.374
Hs Code.:

Synonyms:5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose

Suppliers and Price of 5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

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Technology Process of 5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose

There total 9 articles about 5-Deoxy-1,2-O-(1-methylethylidene)-3-O-(phenylmethyl)-alpha-D-gluco-heptofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89755-56-6
<3aR(3aα,5β,6β,6aα)>-tetrahydro-2,2-dimethyl-5-(2-propen-1-yl)-6-(phenylmethoxy)furo<2,3-d>-1,3-dioxole

: 871347-98-7
(S)-3-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propane-1,2-diol

: 871347-97-6
C₁₇H₂₄O₆

Guidance literature:: With potassium osmate(VI); hydroquinine (anthraquinone-1,4-diyl) diether; potassium carbonate; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 36h;

Reference yield:

: 1-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)-3-hydroxypropan-2-one

: 871347-98-7
(S)-3-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propane-1,2-diol

Guidance literature:: With D-glucose; NAD; potassium carbonate; In aq. phosphate buffer; toluene; at 25 ℃; for 19.5h; pH=7; Reagent/catalyst; Enzymatic reaction;

Reference yield:

: 89755-56-6
<3aR(3aα,5β,6β,6aα)>-tetrahydro-2,2-dimethyl-5-(2-propen-1-yl)-6-(phenylmethoxy)furo<2,3-d>-1,3-dioxole

: 871347-98-7
(S)-3-((3aR,5R,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)propane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; potassium permanganate / acetone; water / 3 h / 0 °C

2: D-glucose; potassium carbonate; NAD / aq. phosphate buffer; toluene / 19.5 h / 25 °C / pH 7 / Enzymatic reaction

With potassium permanganate; D-glucose; NAD; potassium carbonate; acetic acid; In aq. phosphate buffer; water; acetone; toluene;