2-Hydroxycyclohexanone dimer

Base Information

Chemical Name:2-Hydroxycyclohexanone dimer
CAS No.:60308-50-1
Molecular Formula:C12H20 O4
Molecular Weight:228.288
Hs Code.:2932999099
DSSTox Substance ID:DTXSID801222807
Nikkaji Number:J1.801.814D
Mol file:60308-50-1.mol

Synonyms:2-Hydroxycyclohexanone dimer;60308-50-1;1,2,3,4,5a,6,7,8,9,10a-decahydrodibenzo-p-dioxin-4a,9a-diol;dodecahydrodibenzo[b,e][1,4]dioxine-4a,9a-diol;starbld0000684;SCHEMBL1668550;OLLWHBLCQGPTMZ-UHFFFAOYSA-N;DTXSID801222807;J-017855;Octahydrodibenzo[b,e][1,4]dioxin-4a,9a(2H,5aH)-diol

Suppliers and Price of 2-Hydroxycyclohexanone dimer

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Hydroxycyclohexanone dimer

Chemical Property:

Melting Point:100-107 °C(lit.)
Boiling Point:83-86 °C13 mm Hg(lit.)
PKA:11.94±0.40(Predicted)
Flash Point:175 °F
PSA：58.92000
Density:1.297±0.06 g/cm3(Predicted)
LogP:1.29560
XLogP3:0.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:228.13615911
Heavy Atom Count:16
Complexity:254

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s): F,Xi
Hazard Codes:F,Xi
Statements: 11-36/37/38
Safety Statements: 16-26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2(C(C1)OC3(CCCCC3O2)O)O

Technology Process of 2-Hydroxycyclohexanone dimer

There total 7 articles about 2-Hydroxycyclohexanone dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 822-87-7
2-Chlorocyclohexanone

: 60308-50-1,30282-14-5
2-hydroxycyclohexanone dimer

Guidance literature:: With sodium hydroxide; for 12h; Ambient temperature;
DOI:10.1016/S0957-4166(97)00456-4

Reference yield: 30.0%

: 931-17-9
1,2-Cyclohexanediol

: 60308-50-1,30282-14-5
2-hydroxycyclohexanone dimer

Guidance literature:: With pyridine; N-hydroxyphthalimide; sodium perchlorate; In acetonitrile; electrolytical oxidation, anode potential 0.85 V;
DOI:10.1039/c39830000479

Reference yield:

: 1792-81-0
cis-1,2-cyclohexane

: 60308-50-1,30282-14-5
2-hydroxycyclohexanone dimer

: 533-60-8
cyclohexanone-2-ol

Guidance literature:: With [(neocuproine)Pd(OAc)]₂(OTf)₂; oxygen; In water; acetonitrile; at 25 ℃; for 8h; Reagent/catalyst; Overall yield = 81 %; Overall yield = 61 mg;
DOI:10.1021/ja4008694