Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester

Base Information

Chemical Name:Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester
CAS No.:1159977-38-4
Molecular Formula:C₂₇H₂₀O₅
Molecular Weight:424.453
Hs Code.:
Mol file:1159977-38-4.mol

Synonyms:Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester;7-Hydroxy-2,2-diphenyl-1,3-benzodioxole-5-carboxylic Acid Benzyl Ester;7-Hydroxy-2,2-diphenyl-1,3-benzodioxole-5-carboxylic Acid PhenylMethyl Ester

Suppliers and Price of Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
GalicAcid3,4-DiphenylmethyleneKetalBenzylEster
100mg
$ 1110.00

Total 1 raw suppliers

Chemical Property of Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester

Chemical Property:

Melting Point:130-134°C
Boiling Point:609.3±55.0 °C(Predicted)
PKA:8.57±0.40(Predicted)
PSA：64.99000
Density:1.308±0.06 g/cm3(Predicted)
LogP:5.42170
Storage Temp.:Refrigerator
Solubility.:DMSO, Ethyl Acetate

Purity/Quality:: GalicAcid3,4-DiphenylmethyleneKetalBenzylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester

There total 4 articles about Galic Acid 3,4-Diphenylmethylene Ketal Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70475-59-1
3,4,5-triacetoxybenzoyl chloride

: 1159977-38-4
7-Hydroxy-2,2-diphenyl-benzo[1,3]dioxole-5-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N, DMAP / CH₂Cl₂ / 0 deg C, 30 min; room temperature, 4 h

2: 84 percent / K₂CO₃ / methanol; H₂O; CH₂Cl₂ / 0 deg C; room temperature, 1 h

3: K₂CO₃ / acetonitrile / 10 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo961043u

Reference yield:

: 182183-06-8
3,4,5-Triacetoxy-benzoic acid benzyl ester

: 1159977-38-4
7-Hydroxy-2,2-diphenyl-benzo[1,3]dioxole-5-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / K₂CO₃ / methanol; H₂O; CH₂Cl₂ / 0 deg C; room temperature, 1 h

2: K₂CO₃ / acetonitrile / 10 h / Ambient temperature

With potassium carbonate; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo961043u

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1159977-38-4
7-Hydroxy-2,2-diphenyl-benzo[1,3]dioxole-5-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / Et₃N, DMAP / CH₂Cl₂ / 0 deg C, 30 min; room temperature, 4 h

2: 84 percent / K₂CO₃ / methanol; H₂O; CH₂Cl₂ / 0 deg C; room temperature, 1 h

3: K₂CO₃ / acetonitrile / 10 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; In methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/jo961043u