1-AMinoMethyl-1-(Boc-aMino)cyclopropane, 97%

Base Information

• Chemical Name: 1-AMinoMethyl-1-(Boc-aMino)cyclopropane, 97%
• CAS No.: 1027338-34-6
• Molecular Formula: C9H18N2O2
• Molecular Weight: 186.254
• Hs Code.: 2924299090
• Mol file: 1027338-34-6.mol

Synonyms:1-AMinoMethyl-1-(Boc-aMino)cyclopropane, 97%;tert-Butyl 1-(aminomethyl)cyclopropylcarbamate;tert-Butyl N-(1-(aminomethyl)cyclopropyl)carbamate;(1-Aminomethyl-cyclopropyl)-carbamic acid tert-butyl ester

Chemical Property of 1-AMinoMethyl-1-(Boc-aMino)cyclopropane, 97%

Chemical Property:

• Boiling Point: 283.4±9.0 °C(Predicted)
• PKA: 12.74±0.20(Predicted)
• PSA: 64.35000
• Density: 1.06±0.1 g/cm3(Predicted)
• LogP: 2.09360

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl(1-(Aminomethyl)cyclopropyl)carbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-AMinoMethyl-1-(Boc-aMino)cyclopropane, 97%

There total 11 articles about 1-AMinoMethyl-1-(Boc-aMino)cyclopropane, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl [1-(azidomethyl)cyclopropyl]carbamate (849149-60-6) → tert-butyl N-[1-(aminomethyl)cyclopropyl]carbamate (1027338-34-6)

Guidance literature:

With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1002/ejoc.200400599

Reference yield:

C16H24N2O2 → tert-butyl N-[1-(aminomethyl)cyclopropyl]carbamate (1027338-34-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 60 ℃;

Reference yield:

tert-butyl (1-(((diphenylmethylene)amino)methyl)cyclopropyl)carbamate → tert-butyl N-[1-(aminomethyl)cyclopropyl]carbamate (1027338-34-6)

Guidance literature:

With 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol;

upstream raw materials:

tert-butyl [1-(azidomethyl)cyclopropyl]carbamate

tert-butyl (1-(hydroxymethyl)cyclopropyl)carbamate

{1-[(tert-butoxycarbonyl)amino]cyclopropyl}methyl 4-methylbenzenesulfonate

tert-butyl {1-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)methyl]cyclopropyl}carbamate

Downstream raw materials:

4-((1R,3aS,5aR,5bR,7aR,9S,11aR,11bR,13aR,13bR)-3a-((1-(tert-butoxycarbonylamino)cyclopropyl)methylamino)-5a,5b,8,8,11a-pentamethyl-1-(prop-1-en-2-yl)-2,3,3a,4,5,5a,5b,6,7,7a,8,11,11a,11b,12,13,13a,13b-octadecahydro-1H-cyclopenta[a]chrysen-9-yl)benzoic acid

methyl 4-((1R,3aS,5aR,5bR,7aR,9S,11aR,11bR,13aR,13bR)-3a-((1-(tert-butoxycarbonylamino)cyclopropyl)methylamino)-5a,5b,8,8,11a-pentamethyl-1-(prop-1-en-2-yl)-2,3,3a,4,5,5a,5b,6,7,7a,8,11,11a,11b,12,13,13a,13b-octadecahydro-1H-cyclopenta[a]chrysen-9-yl)benzoate

1-Amino-1-(aminomethyl)cyclopropane

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