ethyl 4-broMo-2,6-difluorobenzoate

Base Information

• Chemical Name: ethyl 4-broMo-2,6-difluorobenzoate
• CAS No.: 773139-36-9
• Molecular Formula: C9H7BrF2O2
• Molecular Weight: 265.0514864
• Hs Code.: 2916399090
• Mol file: 773139-36-9.mol

Synonyms:ethyl 4-broMo-2,6-difluorobenzoate

Chemical Property of ethyl 4-broMo-2,6-difluorobenzoate

Chemical Property:

• Vapor Pressure: 0.00198mmHg at 25°C
• Boiling Point: 291.2°C at 760 mmHg
• Flash Point: 129.9°C
• PSA: 26.30000
• Density: 1.573g/cm³
• LogP: 2.90400

Purity/Quality:

99% ^*data from raw suppliers

4-Bromo-2,6-difluoro-benzoicacidethylester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 4-broMo-2,6-difluorobenzoate

There total 1 articles about ethyl 4-broMo-2,6-difluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3,5-difluorobromobenzene (461-96-1) + ethyl cyanoformate (623-49-4) → C9H7BrF2O2 (773139-36-9)

Guidance literature:

3,5-difluorobromobenzene; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at -20 ℃; for 1h; Inert atmosphere; Schlenk technique;

ethyl cyanoformate; In tetrahydrofuran; at 25 ℃; for 1h; Inert atmosphere; Schlenk technique;

DOI:10.1002/adsc.201300185

upstream raw materials:

3,5-difluorobromobenzene

ethyl cyanoformate

Refernces